GCMS reference standard results, Feb 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\FEB1502\REFC.D Vial: 32 Acq On : 16 Feb 2002 11:26 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 20 15:19 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.33 152 281340 20.00 ug/1 -0.02 10) Naphthalene-d8 15.97 136 1078524 20.00 ug/1 -0.02 17) Acenaphthene-dl0 21.29 164 573423 20.00 ug/1 -0.02 29) Phenanthrene-diO 25.73 188 796832 20.00 ug/1 -0.03 38) Chrysene-dl2 33.80 240 516374 20.00 ug/1 -0.04 44) Perylene-dl2 38.08 264 353519 20.00 ug/1 -0.04

System Monitoring Compounds 37) 2,4-DDD 30.81 235 36054 4.51 ug/mL 0.31 Spiked Amount 5.000 Recovery = 90.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.96 74 21130 1.88 ug/1 97 3) bis(2-Chloroethyl)ether 11.72 93 52142 2.82 ug/1 98 4) 1,3-Di chlorobenzene 12.23 146 43594 1.98 ug/1 97 5) 1,4-Dichlorobenzene 12.38 146 46407 2.07 ug/1 98 6) 1,2-Dichlorobenzene 12.89 146 46027 2.16 ug/1 97 7) 2,2'-oxybi s(1-Chioropropan 13.21 45 86513 3.09 ug/1 99 8) N-Nitroso-di-n-propylamine 13.60 70 37966 2.87 ug/1 98 9) Hexachloroethane 13.74 117 14901 1.66 ug/1 92 11) Nitrobenzene 14.02 77 52414 2.36 ug/1 99 12) 1sophorone 14.66 82 108107 2.89 ug/1 99 13) bis(2-Chloroethoxy)methane 15.34 93 65240 2.80 ug/1 99 14) 1,2,4-Trichlorobenzene 15.86 180 40478 2.19 ug/1 96 15) Naphthalene 16.03 128 152574 2.66 ug/1 99 16) Hexachlorobutadiene 16.57 225 17970 1.63 ug/1 97 18) Hexachlorocyclopentadiene 18.77 237 3518 0.43 ug/1 92 19) 2-Chloronaphthalene 19.54 162 92244 2.70 ug/1 99 20) Dimethylphthalate 20.62 163 128742 3.23 ug/1 98 21) 2,6-Dinitrotoluene 20.84 165 18254 2.02 ug/1 95 2 2) Acenaphthylene 20.81 152 137356 2.78 ug/1 98 2 3) Acenaphthene 21.38 153 102197 2.96 ug/1 98 24) 2,4-Dinitrotoluene 22.02 165 23139 2.02 ug/1 98 25) Diethylphthalate 22.76 149 130411 3.15 ug/1 98 26) 4-Chlorophenyl-phenylether 22.92 204 54047 3.03 ug/1 96 27) Fluorene 22.90 166 110048 2.92 ug/1 99 2 8) Azobenzen/ 1,2-Diphenylhyd 23.38 77 122431 2.81 ug/L 98

(#) = qualifier out of range (m) = manual integration REFC.D GCMS0208.M Wed Feb 20 15:21:20 2002 Page 1

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