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GCMS reference standard results, Feb 2002

Machine-extracted title · confidence 95%

Reference standard analysis report for GCMS testing verifying instrument performance with specific compound concentrations.

NYC-WTC_000009716–000009720

Folder label: “GCMS X 1/17/02 A 2/17/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) 4k Data File : C:\HPCHEM\1\DATA\FEB15 02\REFC.D Vial: 32 Acq On : 16 Feb 2002 11:26 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 20 15:19 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.31 168 37701 2.41 ug/1 98 31) 4-Bromophenyl-phenylether 24.39 248 30878 3.06 ug/1 95 3 2) Hexachiorobenzene 24.82 284 35423 3.00 ug/1 99 3 3) Phenanthrene 25.80 178 151793 3.15 ug/1 98 3 4) Anthracene 25.94 178 132476 2.81 ug/1 99 35) Di-n-butylphthalate 27.70 149 191828 2.85 ug/1 99 3 6) Fluoranthene 29.43 202 136104 2.83 ug/1 99 3 9) Pyrene 30.10 202 141780 3.14 ug/1 98 40) Butylbenzylphthalate 32.23 149 51539 2.06 ug/1 96 41) Benzo(a)anthracene 33.75 228 100581 3.04 ug/1 99 42) Bis(2-ethylhexyl)phthalate 34.01 149 76102 2.25 ug/1 99 43) Chrysene 33.88 228 113683 3.49 ug/1 99 45) Di-n-Octylphthalate 35.75 149 68304 1.21 ug/1 # 94 46) Benzo(b)fluoranthene 36.87 252 82478 2.58 ug/1 100 47) Benzo(k)fluoranthene 36.93 252 104465 3.25 ug/1 99 4 8) Benzo(a)pyrene 37.88 252 63336 2.39 ug/1 97 49) Indeno(1,2,3-cd)pyrene 42.29 276 67005 2.77 ug/1 99 50) Dibenz(a,h)anthracene 42.36 278 60070 3.25 ug/1 98 51) Benzo(g,h,i)perylene 43.55 276 66054 3.39 ug/1 96

(#) = qualifier out of range (m) = manual integration REFC.D GCMS0208.M Wed Feb 20 15:21:23 2002 Page 2

NYC-WTC_000009719

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NYC-WTC_000009719Source: NYC Law Department, mirrored locally

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