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GCMS reference analysis results for sample AE02966, February 2002

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Reference analysis report for DEP sample AE02966 showing measured values for target compounds against detection limits.

NYC-WTC_000005614–000005618

Folder label: “GCMS X 2/7/02 A 2/9/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\FEB0 80 2\REFB.D Vial: 29 Acq On 9 Feb 2002 12:32 pm Operator: 209 GALOS Sample GC/MS SCAN 2/7 inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 13 9:33 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Feb 08 15:29:22 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.32 168 49203 2.10 ug/1 97 31) 4-Bromophenyl-phenylether 24.41 248 36507 2.41 ug/1 96 32) Hexachlorobenzene 24.85 284 36491 2.05 ug/1 99 3 3) Phenanthrene 25.82 178 190737 2.64 ug/1 100 3 4) Anthracene 25.95 178 169866 2.40 ug/1 98 35) Di-n-butylphthalate 27.72 149 253010 2.50 ug/1 99 36) Fluoranthene 29.45 202 186009 2.57 ug/1 98 3 9) Pyrene 30.13 202 192674 2.87 ug/1 99 40) Butylbenzylphthalate 32.25 149 75641 2.03 ug/1 92 41) Benzo(a)anthracene 33.77 228 136300 2.78 ug/1 99 42) Bis(2-ethylhexyl)phthalate 34.03 149 99193 1.98 ug/1 99 43) Chrysene 33.90 228 151641 3.14 ug/1 100 45) Di-n-Octylphthalate 35.77 149 97643 1.31 ug/1 # 97 46) Benzo(b)fluoranthene 36.89 252 115544 2.75 ug/1 98 47) Benzo(k)fluoranthene 36.96 252 131699 3.12 ug/1 97 4 8) Benzo(a)pyrene 37.90 252 77806 2.23 ug/1 97 49) Indeno(1,2,3-cd)pyrene 42.32 276 73258 2.31 ug/1 96 50) Dibenz(a,h)anthracene 42.40 278 63595 2.62 ug/1 99 51) Benzo(g,h,i)perylene 43.59 276 68623 2.68 ug/1 99

(#) = qualifier out of range (m) = manual integration REFB. D GCMS0208.M Wed Feb 13 09:41:10 2002 Page 2

NYC-WTC_000005617

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NYC-WTC_000005617Source: NYC Law Department, mirrored locally

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