Reference analysis results for volatile organic compounds analyzed by GCMS on February 8, 2002.
NYC-WTC_000003827–000003831Folder label: “GCMS X 1/28/02 A 2/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\FEB0 802\REFA.D Vial: 16 Acq On 8 Feb 2002 11:55 pm Operator: 209 GALOS Sample GC/MS SCAN 1/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 13 8:23 2002 Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Feb 08 15:29:22 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Compound R.T. Qlon Response Cone Unit Qvalue
30) N-Nitrosodiphenylamine 23.33 168 40951 2.21 ug/1 97 31) 4-Bromophenyl-phenylether 24.41 248 30686 2.56 ug/1 92 32) Hexachlorobenzene 24.84 284 32176 2.29 ug/1 96 33) Phenanthrene 25.82 178 154913 2.71 ug/1 99 34) Anthracene 25.95 178 131867 2.35 ug/1 99 35) Di-n-butylphthalate 27.72 149 237597 2.97 ug/1 99 36) Fluoranthene 29.45 202 143299 2.51 ug/1 100 3 9) Pyrene 30.13 202 148526 2.73 ug/1 99 40) Butylbenzylphthalate 32.25 149 56260 1.87 ug/1 97 41) Benzo(a)anthracene 33.77 228 101547 2.55 ug/1 99 42) Bis(2-ethylhexyl)phthalate 34.03 149 75001 1.84 ug/1 98 43) Chrysene 33.90 228 119843 3.06 ug/1 100 45) Di-n-Octylphthalate 35.78 149 69529 1.09 ug/1 # 97 46) Benzo(b)fluoranthene 36.89 252 87265 2.44 ug/1 98 47) Benzo(k)fluoranthene 36.96 252 96697 2.69 ug/1 98 48) Benzo(a)pyrene 37.91 252 59682 2.01 ug/1 98 49) Indeno(1,2,3-cd)pyrene 42.32 276 60526 2.23 ug/1 97 50) Dibenz(a,h)anthracene 42.41 278 53041 2.56 ug/1 99 51) Benzo(g,h,i)perylene 43.59 276 59861 2.74 ug/1 97
(#) = qualifier out of range (m) = manual integration REFA.D GCMS0208.M Wed Feb 13 08:27:36 2002 Page 2
NYC-WTC_000003830
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Reference analysis report for DEP sample AE02966 showing measured values for target compounds against detection limits.
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Laboratory report listing recovery percentages for thirteen volatile organic compounds in reference standard AE00109 analyzed on February 14, 2002.
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Reference data report for GCMS analysis of sample AE01463 conducted on February 27, 2002.
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Reference analysis report showing measured concentrations of volatile organic compounds in sample AD31662 on February 13, 2002.
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Reference standard analysis report for gas chromatography-mass spectrometry of sample AD29932 conducted on December 18, 2001.
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GCMS reference standard analysis for sample AD28903 dated December 7, 2001, showing measured concentrations.
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Reference standard analysis report for GCMS testing verifying instrument performance with specific compound concentrations.
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Laboratory report listing detection results for volatile organic compounds in reference sample AD31498 analyzed on February 27, 2002.
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Laboratory report of GCMS reference standard analysis for sample AD29665 conducted on December 15, 2001.
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Reference sheet listing expected values and detection limits for volatile organic compounds in WTC samples.
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Laboratory report detailing GCMS calibration analysis for various organic compounds including nitrosamines and chlorobenzenes conducted on December 13, 2001.
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Data sheet recording concentrations of volatile organic compounds analyzed by GCMS on February 8, 2002.
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