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GCMS analysis results for sample AE02603, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE02603 conducted on March 7, 2002, including surrogate recovery data.

NYC-WTC_000005333–000005343

Folder label: “GCMS X 2/5/02 A 3/1/02

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NYC 9/11 Public Portal Document LIDLary bedLCI Lompouru KepoL L

Data File C:\HPCHEM\l\DATA\MAR0102\2603.D Vial: 13 Acq On 1 Mar 2002 8:10 pm Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

25.85 0.24 ug/1 27538 Phenanthrene-dl0 25.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual A/ ---------------------------------------

1 Anthracene-dl0 - 188 C14D10 001719-06-8 72 2 Phenanthrene-diO 188 C14D10 001517-22-2 72 3 Cyclohexanone, phenylhydrazone 188 C12H16N2 000946-82-7 9 4 Pentacyclo [8.4.0.0 (3,7) . 0 (4,14) . 0 (6 188 C14H20 000000-00-0 9 Abundance Scan 2267 (25.855 min): 2603.D (-) m/z 188.10 100.00% 188

5000- /........................ 1 1 । ■ 1 1 1 1 1 ■ ■ ■ । 1 1 ■ 1 i 1 ■ 94 36 80 160 | .____ 25.60 25.80 26.00 26.20 —PP - i ■11 ■ i' 4- i m/z 189. 10 21.06% m/z-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 । Abundance #19957: Anthracene-d10- 188

..................................................... 5000 25.60 25.80 26.00 26.20

80 94 m/z 184.10” 19.15% 160

m/z-> 60 66 ' ' I ' ' ' ' I 1 70 ■ i ■ ■ ■ ■ । । 80 90 1 [ ' 1 ‘ 1 I 1 1 ' 1 I 1 1 1 1 I 1 1 ‘ 1 I 1 1 1 1 I 1 1 1 1 I 1 1 1 1 I ' 1 1 1 I 1 100 110 120 130 140 150 160 170 180 LL 190 Abundance ..................................................... 188

25.60 25.80 26.00 26.20 5000 m/z 94.00 16.97%

80 94 160 66 ' ' i 1 ' ' ■ i ' ' ' ' i ' ' ' ' i 1 1 ' ' i ' ' ' ‘ I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' m/z-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19927: Cyclohexanone, phenylhydrazone ....................... ............................. 188 25.60 25.80 26.00 26.20 93 ; m/z 65.95 11.26%

5000 65 77 106

m/z-- > —TPmmPTt 60 70 80 90 H 100 110 120 132 I N 1 i 1 ' ' ' I ‘ ' 1 ' 1 1 ' ■ ' I ' 1 1 1 i ' ' 111 120 130 140 145

150 159 160 170 170 180 1 , 190 25.60 25.80 26.00 26.20

2603.D GCMS0208.M Mon Mar 04 11:47:39 2002 Page 3

NYC-WTC_000005342

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NYC-WTC_000005342Source: NYC Law Department, mirrored locally

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