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GCMS blank analysis results, Mar 5, 2002

Machine-extracted title · confidence 90%

Laboratory report showing non-detectable results for nitrosamines and chlorinated solvents in GCMS blank.

NYC-WTC_000005507–000005515

Folder label: “GCMS X 2/6/02 A 3/1/02

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Scanned page image, NYC-WTC_000005513
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document L LDL aL y OUaLti tpourru RpUL

Data File C:\HPCHEM\l\DATA\MAR0102\LBA.D Vial: 14 Acq On 1 Mar 2002 9:09 pm Operator: Sample gc/ms scan 2/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.85 0.31 ug/1 39422 Phenanthrene-dl0 25.71

Hit# of 5 Tentative ID MW Mo l Form" CAS# Qual

1 Anthracene -d10- 188 C14D10 001719-06-8 72 2 Phenanthrene-dl 188 C14D10 001517-22-2 72 3 Phosphoni acid, (3-methyl-3-penten 188 C8H13O3P 022152-34-7 50 4 4-Fluoro- -methyl-2-phenylpyrimidin 188 C11H9FN2 000000-00-0 38 Abundance j Scan 2267 (25.852 min): LBA.D (-) ita m/z 188. 10 ' 10 0. 00%

5000 94 ............................. ................. p 80 156

m/z-> .... 44,.... -H L 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 25.60 25.80 26.00 26.20 93.95 22.53% Abundance #19957: Anthracene-dlO- 188

5000 ■ ' I ' ' 25.60 25.80 26.00 26.20 m/z 156.05 17.88% 66 80 34 —mmmPP 160 || m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance 188 ■ ■ i ■ • ‘ 1nr . . । . . . . । . 25.60 25.80 26.00 26.20 5000 m/z 18 10 17.03%

— 94 160 66 93 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19736: Phosphonicacid, (3-methyl-3-penten-i-ynyl)-, dimet 188 25.60 25.80 26.00 26.20 m/z 18 . 10 15.26%

5000 77 62 35 47 93 109 155 1 T‘ 1.1‘I I ■ ■ 1 ] I ■ ■ > j I TTIT ' "I ............................................................. I " 11111, 1111111111111 111 --- m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

LBA.D GCMS0208.M Tue Mar 05 10:55:09 2002 Page 1

NYC-WTC_000005513

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NYC-WTC_000005513Source: NYC Law Department, mirrored locally

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