GCMS blank analysis results, Mar 5, 2002

NYC 9/11 Public Portal Document Library sedrcn Lompounu Kepor L

Data File C:\HPCHEM\1\DATA\MARO102\LBA.D Vial: 14 Acq On 1 Mar 2002 9:09 pm Operator: Sample gc/ms scan 2/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Hexadecane, 1-chloro- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

36.94 0.36 ug/'l 27869 Perylene-d12 38.05

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

l Hexadecane, 1-chloro- 260 C16H33C1 004860-03-1 43 2 2-Ethyl-l-dddecanol 214 C14H30O 000000-00-0 43 3 Cetylpyridinium Chloride 357 C21H40C1NO 006004-24-6 40 4 Octane, l,l'-oxybis- 242C16H340___ 000629-82-3 38 Abundance / Scan 3475 (36.942 min): LBA.D (-) m/z .. 56.95... 100.00% 57 71 43

5000 83 97 112 155 1 1 I 1 ■ ■ ■ f 1 1 ' 1 I ' 1 ' 1 1 1 1 1 1 I

m/z-> । “ ■ 11 30 40 50 60 70 80 4 1’3 I‘ 90 100 110 120 130 140 150 160 | ' I ' " ' L" " I " ' ' | | ‘'I""I'1"I"‘'I“' 170 180 190 200 210 207 36.60 36.80 37.00 37.20 m/ z 71.00 83.21%

Aa Abundance #35935: Hexadecane, 1-chloro- 57 71 91 5000 ■ ■ i ■ 36.60 36.80 37.00 37.20 83 m/ z 55.00 81.38% , 105 ‘1 ‘ ■ I " TT | L i , 133 i11" l " ' 1 I 1 " 11'« ‘ • ‘ I ' ' “ I " ■ ‘ I ■ I ■«I * I I I I 11 n 11 U 11 * I I 11 I n I | I I 111 I I I m z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance 57 ' / ....... "Mww N IIdn/nGIun/nui 71 36.60 36.80 37.00 37.20 5000 m/ z 43.05 72.17% 83 97

WW 111 125 168 196

... M i" " i' ‘ ‘ ‘ i “ " I''' ‘ i" " I ‘‘' i" ' ‘ i " " i ■ “ ‘ i" ■' i" " 11' “ Ir" 111"1111111" " I r‘" I " 111" m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #56020: Cetylpyridinium Chloride E5 ' 1 1 1 ' ' ■ i ■ ' ' ■ i 43 36.60 36.80 37.00 37.20 m/ z 41.00 66.70% 69 91 5000

i" " i 1 ■ i" 83

i, 105 I, l 119 M 133 nuh’i | l l .

m/z-X 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 | . 1 | I I 1 I | 1 I I I | I I 1 1 ] U J I | 1 | | I | ! ! ! | | | | ! | | ! | _any 36.60 36.80 37.00 37.20

LBA.D GCMS0208.M Tue Mar 05 10:55:14 2002 Page 2

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