Calibration data for GC/MS analysis of surrogate compounds including dichlorobenzenes and naphthalene from April 2002.
NYC-WTC_000043699–000043713Folder label: “GCMS X 4/24/02 A 5/3/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document LLDLdry bedICI LoIpOUru KepOIC
Data File : C:\HPCHEM\ 1\DATA\APR2 302\8837.D Vial: 6 Acq On : 23 Apr 2002 7:18 pm Operator: Sample : gc/ms scan 4/15 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 6 N-Acetylpyrrolidone Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
8.25 1.57 ug/1 225549 1,4-Dichlorobenzene-d4 12.22
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 9 2 Pentacosane 352 C25H52 000629-99-2 9 3 2 -Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 9 4 Heptacosane 380 C27H56 000593-49-7 9 Abundance Scan 349 (8.250 min): 8837.D (-) m/ z 43.05 100.00% 43
5000
— 125 r-r 1 1 1 1 ------—— , 63 82 99 I 8.00 8.20 8.40 8.60 al AL Illi III II ill ’ ’’I’ TT 1’111"5"T7’171111117171171171111’1’1"1T7TTT’’’’0’111T r 111111" i1' " i m/z 124.80 17.45% mlz->20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #4732: N-Acetylpyrrolidone 43
.w i1111।■‘' 5000 8.00 8.20 8.40 8.60 99 127 m/z 126.90 12.22%
m/z-> T" III I__ I 49.4. Tn ' 11 > - -1 ■ - - - । -1 < > " । " - ■ [ । 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 । [ I'''11''11111 " I
Abundance #49559: Pentacosane 43 ..... 1...... 1 ' ' 1 1 1 1 1 1 r ‘ 1 1 1 1 1 1 1'I 1 1 1 71 8.00 8.20 8.40 8.60 5000 m/z 81.85 10.56%
, 99 0+ ■111 " ' i I; Ik i । 127 197 225 253 325 352 I •'1' IT u 111' 1‘110111—0010010TT—T7100011005011—01IUB—ICCTDTtTT m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #12247: 2-Propanone, 1,1,1 -trichloro- ......... .... ........ I I I I I I I I I I I I I I I I I I I I I I I 43 8.00 8.20 8.40 8.60 m/z 46.90 9.98% 5000
15 14 85 125 । '* | I1 । । i' | । >' । | i' 'i ' । | । I i [ I i I r [ • f I I | I I I r | I | I I | J I I I |“I IT I | I ! I I | I I | I | I r I I | t J l' I |" NAApaALAAAA A m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 8.00 8.20 8.40 8.60
8837.D GCMS0412.M Wed Apr 24 08:36:39 2002 Page 6
NYC-WTC_000043710
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NYC-WTC_000043146
Laboratory document displaying a GCMS calibration table with retention times and response factors for deuterated standards from May 2002.
1 shared topics · Same agency, volume and box · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045526
GC/MS instrument calibration report for polycyclic aromatic hydrocarbons and chlorinated compounds using 40 µg/L standards, dated May 2-3, 2002.
1 shared topics · Same agency, volume and box · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043164
Laboratory report for DEP Box 25 showing GCMS blank analysis of sample AE09450 with semi-volatile organic compounds below detection limits from May 3, 2002.
Same agency, volume and box · similarity 0.983
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043079
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09393 with unknown compounds and surrogate data from May 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.982
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043238
Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.
1 shared topics · Same agency, volume and box · similarity 0.982
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043678
Calibration table for GC/MS analysis listing deuterated standards and their response values from April 24, 2002.
Same agency, volume and box · similarity 0.981
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038801
Laboratory report detailing analysis of unknown compounds and surrogate recovery for sample AE02460.
1 shared topics · similarity 0.982
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011800
Laboratory report documenting GCMS analysis of environmental sample AE04129 conducted on April 1, 2002.
1 shared topics · similarity 0.982
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048583
Instrument calibration records and method parameters for GCMS analysis of polycyclic aromatic hydrocarbons.
1 shared topics · similarity 0.982
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005545
Gas chromatography-mass spectrometry analysis of sample AE02785 performed on 3/11/2002, detecting 2,4-DDD and other unknown compounds.
1 shared topics · similarity 0.982
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052832
GC/MS analysis report for sample AE01043 showing surrogate recovery data generated on February 25, 2002.
1 shared topics · similarity 0.982
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011817
Laboratory report documenting GCMS analysis of environmental sample AE04131 conducted on April 1, 2002.
1 shared topics · similarity 0.981
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NYC-WTC_000043641
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 24 and May 3, 2002.
Filed in the same folder
NYC-WTC_000043642
Technical record of GC/MS analytical parameters and sample processing details for the batch dated May 2002.
Filed in the same folder
NYC-WTC_000043646
Laboratory report documenting a GC/MS blank run to check for contamination in the analytical system on May 6, 2002.
Filed in the same folder
NYC-WTC_000043655
Calibration report listing target compounds and their concentrations for the GC/MS analysis performed on May 6, 2002.
Filed in the same folder
NYC-WTC_000043659
Report detailing the response values for GC/MS reference standards used to verify instrument performance on May 6, 2002.
Filed in the same folder