Calibration data for GC/MS analysis of surrogate compounds including dichlorobenzenes and naphthalene from April 2002.
NYC-WTC_000043699–000043713Folder label: “GCMS X 4/24/02 A 5/3/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Llprary bearen compound Keporc
Data File : C : \HPCHEM\ 1\DATA\APR2 302\8837.D Vial: 6 Acq On : 23 Apr 2002 7:18 pm Operator: Sample : gc/ms scan 4/15 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
8.19 4.95 ug/1 710514 1,4-Dichlorobenzene-d4 12.22
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 50 2 Acetic acid, 1,1-dimethylethyl este 116 C6H1202 000540-88-5 33 3 Acetone/ 58 C3H60 000067-64-1 9 4 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 9 Abundance ( Scan 342 (8.185 min): 8837. D (-) m/z 43.00 100.00% 43
59 5000
101 ........................... 1 i ■ ■ 7.80 8.00 8.20 8.40 8.60 .................... ... 1ki।itpiiii।iiii।r 1 -P 53 , 71 83 i ' 1 ■ ' i ' 1 1 ■ i ' 1 ' ' i 1 m/ z 59.05 50.69% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 43
I | t t I I | I I I T ] I I i — I I I I [ I t 5000 59 7.80 8.00 8.20 8.40 8.60 m/z 101.05 21.38% 15 31 . 101 83 | 111 .... . IIIIIIIIIIIIIIIIIIIIIII* m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3292: Acetic acid, 1,1 -dimethylethyl ester 43 III ii 1 । 1 1 1 ' 1 7.80 8.00 8.20 8.40 8.60 5000 57 m/z 58.00 16.18% 101 15 27 TT 1.......... ■ । 1 1 * 1 । 1 ■ । * । > 1 < । । > ■ 1 1 । > > । ■ । , n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #94: Acetone ------------------------ 43 7.80 8.00 8.20 8.40 8.60 m/z 41.00 7.89%
5000 15 58 27 ------ 1 ■ ■ i 1 ■ i ' 1 1 1 i 1 ■ r 1 i ' 1 1 ' i 1 1 ' 1 1 1 1 1 1 1 1 ' I 1 ■Vr ! I,nu ' ■T1-1 *' i | 1-1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60
8837.D GCMS0412.M Wed Apr 24 08:36:38 2002 Page 5
NYC-WTC_000043709
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NYC-WTC_000043146
Laboratory document displaying a GCMS calibration table with retention times and response factors for deuterated standards from May 2002.
1 shared topics · Same agency, volume and box · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045526
GC/MS instrument calibration report for polycyclic aromatic hydrocarbons and chlorinated compounds using 40 µg/L standards, dated May 2-3, 2002.
1 shared topics · Same agency, volume and box · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043164
Laboratory report for DEP Box 25 showing GCMS blank analysis of sample AE09450 with semi-volatile organic compounds below detection limits from May 3, 2002.
Same agency, volume and box · similarity 0.983
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043079
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09393 with unknown compounds and surrogate data from May 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.982
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043238
Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.
1 shared topics · Same agency, volume and box · similarity 0.982
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043678
Calibration table for GC/MS analysis listing deuterated standards and their response values from April 24, 2002.
Same agency, volume and box · similarity 0.981
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038801
Laboratory report detailing analysis of unknown compounds and surrogate recovery for sample AE02460.
1 shared topics · similarity 0.982
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011800
Laboratory report documenting GCMS analysis of environmental sample AE04129 conducted on April 1, 2002.
1 shared topics · similarity 0.982
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048583
Instrument calibration records and method parameters for GCMS analysis of polycyclic aromatic hydrocarbons.
1 shared topics · similarity 0.982
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005545
Gas chromatography-mass spectrometry analysis of sample AE02785 performed on 3/11/2002, detecting 2,4-DDD and other unknown compounds.
1 shared topics · similarity 0.982
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052832
GC/MS analysis report for sample AE01043 showing surrogate recovery data generated on February 25, 2002.
1 shared topics · similarity 0.982
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011817
Laboratory report documenting GCMS analysis of environmental sample AE04131 conducted on April 1, 2002.
1 shared topics · similarity 0.981
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NYC-WTC_000043641
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 24 and May 3, 2002.
Filed in the same folder
NYC-WTC_000043642
Technical record of GC/MS analytical parameters and sample processing details for the batch dated May 2002.
Filed in the same folder
NYC-WTC_000043646
Laboratory report documenting a GC/MS blank run to check for contamination in the analytical system on May 6, 2002.
Filed in the same folder
NYC-WTC_000043655
Calibration report listing target compounds and their concentrations for the GC/MS analysis performed on May 6, 2002.
Filed in the same folder
NYC-WTC_000043659
Report detailing the response values for GC/MS reference standards used to verify instrument performance on May 6, 2002.
Filed in the same folder