Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.
NYC-WTC_000043378–000043384Folder label: “GCMS X 4/23/02 A 4/24/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\APR1802\7002.D Vial: 20 Acq On : 19 Apr 2002 6:30 am Operator: Sample : GC/MS SCAN 3/26 FB Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T. 8.21 50.64 ug/1 8554770 1,4-Dichlorobenzene-d4 12.21 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 72 2 Acetic acid, 1,1-dimethylethyl este 116 C6H1202 000540-88-5 33 3 Acetic acid, cyano-, 1,1-dimethylet 141 C7H11NO2 001116-98-9 17 4 CH2=CHCH2C(O)OCH3 100 C5H802 003724-55-8 10 Abundance / Scan 345 (8.210 min): 7002.D (-) m/z 42.95 100.00% 43
59 5000
101 ■ ■ i 1 ■ ■ ' i ■ 1 ‘TI । । । । । । । 7.80 800 8.20 8.40 8.60
mlz-> + WTTp 69 83 ’T , 207 116 i1"11" " ।"111 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 i" " i" " r ■ ‘' r "' r1111"' ’ i" " I" " i' m/ z 59.05 51.17% Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43
5000 59 7.80 8.00 8.20 8.40 8.60 m/z 100.95 21.65% 27 - TTTT . 83 .. I101... i" " r "1 r1111 ।" “ i11" ।।।। " i" " i" " i" " i mlz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #3292: Acetic acid, 1,1 -dimethylethyl ester 43 ET ’ 1 i ' 1 r 1 i ‘ 1 i 1 1 1 ■ i 1 1 7.80 8.00 8.20 8.40 8.60 5000 57 m/z 58.05 16.27% 101 15 27 i i | i i i i | i i ii । TTTT i " " I " " I"1' r "11 ‘' i'1" r1 " i" " i" " i I" •' i" " i" " i m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #7666: Acetic acid, cyano-, 1,1-dimethylethyl ester 59 7.80 8.00 8.20 8.40 8.60 m/z 41.05 7.88% 5000 41
126 ।" " । i" " r11' r "1 r1 । । । । 1 । 1 1 ' * । 1 1 1IIIIIII T m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 7.80 8.00 8.20 8.40 8.60
7002.D GCMS0419.M Mon Apr 22 08:32:53 2002 Page 1
NYC-WTC_000043383
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NYC-WTC_000043482
Gas chromatography-mass spectrometry analysis report for sample AE07107 including surrogate compound recovery data.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045490
Technical document displaying GCMS calibration data and compound retention times for sample AE09448 processed in early May 2002.
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Technical document displaying GCMS calibration data and compound retention times for sample AE09447 processed in early May 2002.
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Gas chromatography-mass spectrometry analysis report for sample AE07067 including surrogate compound recovery data.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022902
Reviewed data file listing retention times and response factors for deuterated internal standards.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022780
Reviewed data file listing retention times and response factors for deuterated internal standards.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023828
Laboratory report of GCMS analysis for sample AE09680 conducted on May 23, 2002, showing surrogate recovery data.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023754
Laboratory report of GCMS analysis for sample AE09654 conducted on May 23, 2002, showing surrogate recovery data.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013251
Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023701
Laboratory report of GCMS analysis for sample AE10063 conducted on May 23, 2002, showing surrogate recovery data.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023738
Laboratory report of GCMS analysis for sample AE10065 conducted on May 23, 2002, showing surrogate recovery data.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023684
Laboratory report of GCMS analysis for sample AE10062 conducted on May 23, 2002, showing surrogate recovery data.
1 shared topics · similarity 0.995
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NYC-WTC_000043329
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 23 and April 24, 2002.
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NYC-WTC_000043330
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NYC-WTC_000043332
Laboratory report documenting GCMS blank analysis for multiple organic compounds on April 24, 2002.
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NYC-WTC_000043340
Calibration verification records for gas chromatography-mass spectrometry analysis of volatile organic compounds.
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NYC-WTC_000043344
Reference standard analysis data for volatile organic compounds obtained via gas chromatography-mass spectrometry.
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