GCMS analysis results for sample AE02603, Mar 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR0102\2603.D Vial: 13 Acq On 1 Mar 2002 8:10 pm Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L

Peak Number 2 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.20 0.38 ug/1 30768 1,4-Dichlorobenzene-d4 12.31

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentano 1, 3-methyl- 102 C6H140 000077-74-7 36 2 N-Ethylformamide 73 C3H7NO 000627-45-2 4 3 Formic acid, ethyl ester 74 C3H602 000109-94-4 4 4 Norleuine, ethyl ester 159 C8H17N02 006141-42-0 4 Abundance Scan 344 (8.201 min): 2603.D (-) ■ m/z 73.00 100.00%: 73

5000

m/z-> ’ I’ 10 20 30 40 43

50 60 70 80 57.. , , +Pmr ■ 1 87 । 103 1 7.80 m/ z 43.05 ■ 8.00 ■ 8.20 8.40 8.60 ' । 28.56% ■

90 100 110 ■ ■ i ■ ■ L Abundance #63573: 3-Pentanol, 3-methyl- 713

5000 _ 7 80 8.00 8.20 8.401 8.60 55 m/z ’ 44.95 12.01% 45 87 27 39 ■ 'i 1 ■ ■ ' । ■ 1 ■ 1 । ' 1 ■ ■ । ■ ■ ■ ■ ......................... ■ ■ ■ ■ । ■

m/z-> 10___ 20 30 40 50 60 70 80 90 100 110 Abundance 30 73 7.80 8.00 8.20 8.40 8.60 5000 m/ z 41.05 11.80% 44 58

15 I1IIIIFIII m/z-> 10 20 30 40 50 60 70 80 90 100 110 A Abundance #62550: Formic acid, ethyl ester ' - 31 7.80 8.00 8.20 8.40 8.60 | m/z 39.05 6.40% 5000

45 26 - 56 74 | I 1 ' I ' ' ' ' I ' ' ' ' I ' ' ' ‘ I ' ' ' ' I 1 ‘ ' I ' 1 1 ' I ' I • | 1 ’ 1 ' । । । I1' । । ' | । 1 ■ > | 1 ' ; m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

2603.D GCMS0208.M Mon Mar 04 11:47:34 2002 Page 2

NYC-WTC_000005341