GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB05\30644A.D Vial: 1 Acq On 5 Feb 2002 2:56 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 5.92 0.22 ug/L 157518 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 40 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 40 3 1,3-Dioxolane, 2-(3-bromo-5,5,5-... 352 C10H16BrC13O2 000000-00-0 23 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 223 (5.920 min): 30644A.D (-) m/ z 73.10 100.00% 73

5000 43 ' ' i ' ' ' ‘ i ■ 1 •17’’4 L 5.60 5.806.00 6.20 o1 ।' " i ■ d’87 .........Ill , fhhonid 103 I’ 10**** m/ z 43.10 25.21%

I miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 —fri Pi ppi n 5.60 5.80 6.00 6.20 43 m/z 45.10 9.20% 27 55 , 87 113 174 0-TTTT ’111111111111 TI,m—/—nu—O—mTTu1u n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 A.. ) AAA ' rl 1 1 ' ' I 1 1 1 1 ! 5.60 6.00 5.80 6.20 5000; m/z 41.10 8.76% 43

m/z-> 0- + 27 ■ i 55 , 87 113 TP 11" r " ' i " ■ ■ i " " i " ■ ■ i " ■ ■ i174 ■ i ■ ■ ■ ■ i1 Tn-pr 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 '11 ■ i ■

Abundance #299410:1,3-Dioxolane, 2-(3-bromo-5,5,5-trichIoro-2,2-dim... _AAA_ ■ ■ I ■ ■ ■ • i ■ ■ ' ' i 73 5.60 5.806.00 6.20 m/z 71.10 7.06% 5000

45 36 , m/z—> 0 . illeenas 20 30 40 55 ! 109 TTTTITTTTTT *unanuummmmmOg 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

30644A.D SCAN508.M Fri Feb 22 11:44:24 2002 Page 6

NYC-WTC_000004905

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