GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB05\30644A.D Vial: 1 Acq On 5 Feb 2002 2:56 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 2-Propanone, 1,1,1-trichlor... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

6.00 0.08 ug/L 56743 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- (C... 160 C3H3C130 000918-00-3 42 2 1-Fluorononane $$ n-Nonyl fluori... 146 C9H19F 000463-18-3 40 3 2-Propanone, 1,1,1-trichloro- (C... 160 C3H3C130 000918-00-3 40 4 Octan-2-one, 3,6-dimethyl- 156 C10H20O 000000-00-0 28 Abundance Scan 230 (5.999 min): 30644A.D (-) m/z 43.10 100.00% 43

5000

97 127 ’ .. J ,, 51 61 83 5.60 5.80 6.00 6.20 6.40 0 0 W1'1 i’i'i > 11111111 ‘ 1111 t'l111 i ' 1 ' 11■ i । ■ ■ ■ । 1 ■ ■ ■ i 1 ''11 1 i ■ ■ m/z 83.00 11.42% nz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #59078:2-Propanone, 1,1,1-trichloro- (CAS) $$ Trichloroac... 43

5000 5.60 5.80 6.00 6.20 6.40 m/z 126.90 8.97% 61 82 97 35 49 117 125 01 ■ ' I 1 ' 1 ' 1 1 1 1 ‘ 1 1 1 1 1 I 1 1 1 1 1 1 1 ■ 1 I1' 1 1 1 I rr 'l1 1,1 ■ ।1 ■ ■ ■ । ■ ■ ■ • । ‘ ■ ■ ■ ।' ■1' i ■ ■ n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #42575:1-Fluorononane $$ n-Nonyl fluoride $$ Nonane, 1 -fl... 43 5.60 5.80 6.00 6.20 6.40 5000 m/z 125.00 8.96% 56 27 70 84 97

0- ' ■ i ■ ' ‘ ' i ' ' ' ' i 33 ' i ■| ‘ i ■ ■ T-p-r 1.. . ...... ■ ■ i 1 1 ■1 i 1 ‘ ■ i ■ 1' 1 1 1 1 ' 1 1 1' n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #59082:2-Propanone, 1,1,1-trichloro- (CAS) $$ Trichloroac... 43 5.60 5.80 6.00 6.20 6.40 m/z 97.00 8.60% 5000

m/z-> 15 I 20 27 0 ‘ 1+1′4111111′4111 10 30 40 , 49 63 85 97, 110 117 127 ’ i ■ > i ■ ■ • ■ r- ■ । ■ । ■ ■ ■ ■ । *'1 ■ । • * ■ ■ । 114****.. 11.. 50 60 70 80 90 100 110 120 130 ........ H........ 5.60 5.80 6.00 6.20 6.40

30644A.D SCAN508.M Fri Feb 22 11:44:24 2002 Page 7

NYC-WTC_000004906

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