GCMS DFTPP calibration report, Feb 5 2002

Machine-extracted title · confidence 95%

Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB05\30644A.D Vial: 1 * Acq On 5 Feb 2002 2:56 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library- : C: \DATABASE\WILEY7N . L ********************************************************************* Peak Number 6 2-Propanol, 1-(2-methoxy-l-... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

9.55 0.08 ug/L 58705 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methy... 148 C7H1603 020324-32-7 78 2 2-Propanol, 1,1'-oxybis- (CAS) $... 134 C6H14O3 000110-98-5 39 3 E-Dipropylene glycol $$ 2-hydrox... 134 C6H14O3 000000-00-0 36 4 Butyl aldoxime, 3-methyl-, syn- 101 C5H11NO 005780-40-5 23 Abundance Scan 541 (9.550 min): 30644A.D (-) m/z 59.10 100.00% 59

5000- 45 73

0 । . . . . । . . . . । 111, i ।11 । । । ■ । । L । l । . ' 1 . । . 86 103

9.20 m/z .N ' ' I ' ' 1 ‘ I ' ' ' ' 1 1 1 ' ' 1 1 9.40 9.60 45.10 9.80 44.84%

UA i ■ ' ' 1 i ■ • /z—> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #43943:2-Propanol, 1-(2-methoxy-1-methylethoxy)- $$ Dipro... 59

5000 45 103 9.20 9.40 9.60 9.80 73 31 m/z 103.10 37.83% A ..................... 130 O- 1 1 i ''' ■ > । I ''i > । > । । I............... M. m/z-> 20 30 40 50 (60 70 80 90 100 110 120 130 Abundance #29204:2-Propanol, 1,1 ’-oxybis- (CAS) $$ Dipropylene glyc... 59 —

9.20 9.40 9.60 9.80 31 m/z 73.10 28.58% 5000 45 103

i ■ ■ ■ , ' ' ■ i 0 TT ' 1 i । > • > ■ । > ■ ■ ■ i ■ ■ > • i ■ ■ ■ ■ 1 • i • > i ' ■ > > i ■ ■ ■ ■ । ■ m/z-> 20 Abundance 30 40 50 (60 70 80 90 100 110 120 #29239: E-Dipropylene glycol $$ 2-hydroxyethyl ether 130 ... AN \ — ' 1 i ■ ■ ■ ■ i 1 ■ ■ 1 । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ 31 59 9.20 9,40 9.60 9.80 m/z 41.10 27.05%

5000 45 103 39 75 0 ..................... r 1 11 i1 1 1 1 । I ........ 'Up.,. ■ i ■ ■ i ' 1 ' ' i ' ‘ ' i ' 1 ' 1 i ' ■ 1 ' i ■ ■ ■ ■ i 1 1 1 1 i 1 ' ■ 1 । ■ 1 r■ 1 ■ ■ । ' 1 ■ । 1 m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 9.20 9.40 9.60 9.80

30644A.D SCAN508.M Fri Feb 22 11:44:24 2002 Page 8

NYC-WTC_000004907

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NYC-WTC_000004907Source: NYC Law Department, mirrored locally

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