Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\LBD.D Vial: 38 Acq On : 29 Dec 2001 7:39 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
30.25 0.38 ug/1 130154 Chrysene-dl2 33.02
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7yHeptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 42 2 1 -Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 36 3 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 28 4 Di thioerythritol, tetrakis (trimethy 44 2 Cl6H42 02S2 Si4 000000-00-0 23 Abundance Scan 2746 (30.251 min): LBD.D (-) m/ z 73.00 100.00% 73
j 5000 147 221 • Y . [ > Si . | i . . , । . | 281 355 420 30.00 30.20 30.40 30.60 45 117 1 I j i191 L 249 I 325. [ 401 i ■ '“T' 1 T ’ 11 ] rh 1 — H j l i । । i ’ । t i [ 1 ! i 1 ] i i i i ] i r m/ z 147.00 36.80% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #56714: 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73
147 5000 267 355 429 30.00 30.20 30.40 30.60 45 207 m/z 221.05 20.42% ' 1 I 1 1 .... H... I,., 1 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolmoleoylgycerol trimethylsily! ether 73 ■ ' i 1 1 ‘ I’’ 30.00 30.20 30.40 30.60 207 5000 147 m/z 355.05 13.76% 34 103 281 1 . I . . 395. .482. 50 100 150 200 250 300 350 400 450 500 550 - Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73 30.00 30.20 30.40 30.60 m/z 281.00 12.85% 5000 147
221 281 327 415 519 501 - i 1 1 ' ' i ' ' miz-> 50 100 150 200 250 300 350 400 450 500 550 30.00 30.20 30.40 30.60
LBD.D GCMS1126.M Mon Jan 28 11:39:37 2002 Page 9
NYC-WTC_000004205
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
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