DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\LBD.D Vial: 38 Acq On : 29 Dec 2001 7:39 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

28.65 0.30 ug/1 152846 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-1, 2,1,7, 7,7-hexamethyl 576 C18H5207Si7 071579-69-6 42 2 1-Monolinoleo glycerol trimethylsi 498 C27H5404Si2 054284-45-6 36 3 N-Methyladrenaline, tri-TMS 413 C19H39NO3Si3 000000-00-0 25 _ 4 3~ (2-Methoxyphenox y) lactic acid, di 356 C16H2805Si2 000000-00-0 17 Abundance Scan 2572 (28.654 min): LBD.D (-) m/ z 73.00 100.00% 73

5000 147 355 ■ > i • • • • i ■ ■ i • i ■ > ■ ■ । t 221 281 28.40 28.60 28.80 29.00 45 117 191. 1 1 1) I 1'' Bin 'I1 f 251,■ ■ ’ ' i ■ .401 429 ..... l' f' 1 I 327 . m/z 147.00 33.71% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 147 28.40 28.60 28.80 29.00 221 281 30- m/z 221.05 18.85% -- 415 519 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #588/1: 1-Monolinoleoylglycerol trimethylsilyl ether 73 - 28.40 28.60 28.80 29.00 207 5000 147 16.46% 34 103 ' 281 . i ..... ... 395 ..482. m/z-> 50 100 150 200_ 250 300 350 400 _450 500 550 Abundance #54808: N-Methyladrenaline, tri-TMS ’ 73 28.40 28.60 28.80 29.00 m/z 281.00 13.56% 5000 355 45 . 207 267 ! I — 323 ■ ■ 1 1 1 / m/z-> 50 100 150 200 250 300 350 400 450 500 550 28.40 28.60 28.80 29.00

LBD.D GCMS1126.M Mon Jan 28 11:39:32 2002 Page 8

NYC-WTC_000004204