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GCMS analysis results, sample AD30936, January 2002

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis of sample AD30936 conducted on 1/28/2002, measuring organic compounds including surrogates and unknown compounds.

NYC-WTC_000018775–000018794

Folder label: “GCMS X 12/19/01 A 1/2/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2502\30936A.D Vial: 3 Acq On : 25 Jan 2002 11:09 am Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 3-1sopropoxy-1,1,1,7,7,7-hexam Concentrat ion Rank 10

R.T. EstConc Area Relative to ISTD R.T.

28.45 0.30 ug/1 112740 Phenanthrene-dl0 24.75

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-1,1,1,,7, 7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 1-Monolinoleoylg cerol trimethylsi 498 C27H54O4Si2 054284-45-6 33 3 N-Methyladrenaline, tri-TMS 413 C19H39NO3Si3 000000-00-0 25 4 Benzoic acid 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 25 Abundance Scan 2550 (28.453 min): 30936A.D (-) m/z 73.0,0 100.00% 73

5000 147 221 T I ■ ■ -r-p-r-r-r-p-r 281 355 28.20 28.40 28.60 28.80 45 miz-> ‘1 I r‘r fr 101 50 100 -191.1.1191k 150 249 [ 1 1 1 f ’’I 325 | 401 429 II/A14***‘IIII1I 200 250 300 350 400 450 500 550 m/z 147.00 33.33% Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 147 28.20 28.40 28.60 28.80 221 281 29- A4E m/z 221.05 16.53% 1 miz-> 11 200 50 300 . 415.. 100 450 519150 250 350 400 500 561 1 i r 1 550 Abundance #58871: 1-Monolinoleoyiglycerol trimethyisilyl ether 73

207 28.20 28.40 28.60 28.80 5000 147 m/z 355.0! 14.14% 34 103 281 395 482 i miz-> 50 100 150 200 250 300 350 *400 450 500 550 (Abundance #54808: N-Methyladrenaline, tri-TMS T T T 73 28.20 28.40 28.60 28.80 m/z 281.10 11.56% 5000 355 45 207 267 323 ............. Ms 50 100 150 200 250 T T T T 300 350 400 450 500 550 28.20 28.40 28.60 28.80

30936A.D GCMS1126.M Fri Jan 25 12:24:22 2002 Page 10

NYC-WTC_000018791

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NYC-WTC_000018791Source: NYC Law Department, mirrored locally

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