GCMS analysis results, sample AD30936, January 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2502\30936A.D Vial: 3 Acq On : 25 Jan 2002 11:09 am Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************** Peak Number 11 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

30.05 0.38 ug/1 98821 Chrysene-d12 32.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy-1,1,1.X, 7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 40 2 l,l,l,5,7,7,7-Hep€amethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 36 3 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 23 4 Silanamine, NA[2,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 9 Abundance Scan 2724 (30.050 mln): 30936A.D (-) m/ Z 73.00 100.00% i 73

5000 147 221 ■ ■ 1911 ,L , . . 327.355. 4014?°.. 45 „ I 281 29.80 30.00 30.20 30.40 117 TT ■ • । ■ T-r-r m/z 147.00 35.54% miz-> 50 100 150 ‘ ' 200 ' 250 ‘ 300 350 400 450 500 550 Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-trls(trim 73

5000 —IAr ■ • i • • 147 29.80 30.00 30.20 30.40 221 281 327 m/z 221.0 18.06% 415 519 561 • ■ i ■ ■ • • i • ■ ■ ' i 1 • • ' i • r ■ • i • • 1 i 1 ; i ■ • 1 • i ■ ■ ■ ‘ i ■ • ■ • i • ' ' 1 i 1 1 miz-> 50 100 150 200 250 300 350 400 450 500 550 •Abundance #56714: 1.1.1.5,7.7.7-Heptamethyl-3.3-bis(trimethylsiloxyit 73 -r-r-p-r r' i 1 1»1 r1 1 147 29.80 30.00 30.20 30.40 5000 267 m/z 281.00 10.86% 355 429 45 , • 207

■ ' i • ‘ ■ i ■ • ■ ■ i ■ • ' ‘ i ■ ■ • ■ i ■ ■ ■ 1 l 1 1 ' r 1 1 ' ' 1 1 1 ' 1 I 1 1 1 1 I 1 1 1 1 1 1 1 miz-> 50 100 150 200 250 300 350 4(X) 450 500 550 ... Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73 29.80 30.00 30.20 30.40 m/z 355.0 9.64% 207 5000 147 34 103 281

m/z-> ■ ■ i • ■ 50 100 150 200 250 300 350 395,....482. 400 450 500 550 29.80 30.00 30.20 30.40

30936A.D GCMS1126.M Fri Jan 25 12:24:27 2002 Page 11

NYC-WTC_000018792