DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN25 02\3 0 64 9.D Vial: 34 Acq On : 25 Jan 2002 9:55 pm Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 1-Monolinoleoylglycerol trimet Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

32.88 2.53 ug/1 1386030 Chrysene-dl2 32.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 l 054284-45-6 45 3-Isopropoxy-1,1,1,7/7,7-hexamethyl 576 C18H5207Si7 2 071579-69-6 40 Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 3 018294-04-7 32 2-Hexenedioic acid, bis(trimethylsi 288 C12H2404Si2 4 055494-10-5 23 Abundance Scan 3032 (32.882 min): 30649.D (-) m/z 73.0,0 100.00% 73

5000 147 221 ■ ■ i ■ ■ 281 355 32.60 32.80 33.00 33.20 45 0- TTTT -11—1911.249- L ,327, ... 401 4?% ! ............................... m/z 147.00 41.85% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether ii 73

207 5000 147 32.60 32.80 33.00 33.20 34 103 | 281 m/z 221.05 24.98% I il l L300 350 400 450 500 550 ’’I I 395 482 m/z-> 50 100 150 200 250 Abundance #60503, 3-Isopropoxy-1.1.1.7. f .7-hexamethyl-3,5,5-tris(trim 73

32.60 32.80 33.00 33.20 5000 m/z 281.00 14.84% 147 221 281 327 415 519 561 m/z-> 50 100 150 200 250 300__ 350 400 450 500 __ 550 Abundance #30580: Ethanedioic acid, bis(trimethylsilyl) ester 73 147 32.60 32.80 33.00 33.20 m/z 355.00 13.92% 5000 45

■ • i ■ ■ ■ • i ■ • 190 219 .... । » 1 | । » । । I r । ’ *7 1 ■ i ' ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 32.60 32.80 33.00 33.20

30649.D GCMS1126.M Mon Jan 28 12:18:56 2002 Page 14

NYC-WTC_000004267