DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \HPCHEM\1\DATA\JAN2502\30649.D Vial: 34 Acq On : 25 Jan 2002 9:55 pm Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 15 1-Monolinoleoylglycerol trimet Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

34.18 1.86 ug/1 1021120 Chrysene-dl2 32.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 45 2 Ethanedioic acid, bis(trimethylsily 234 C8H1804Si2 018294-04-7 38 3 9,12,15-Octadecatrienoic acid, 2,3- 496 C27H5204Si2 055521-22-7 23 4 Butanoic acid. 3 -/ethyl-2-[(trimeth 262 CllH26O3Si2 055124-92-0 23 Abundance Scan 3173 (34.176 min): 30649.D (-) m/z 73.00’ 100.00% 73

5000 147 221 FTPPITTT 1 1 i ' 281 355 . 33.80 34.00 34.20 34.40 34.60

m/z-> 0- 45 ■'I 1 ' 96 117 100 +1914 249—3274140144— m/z 147.00 48.68% 50 150 200 250 300 350 400 450 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000- 147 11001 1 1 i 1 i I ' 1 i ' 33.80 34.00 34.20 34.40 34.60 34 103 m/z 221.05 28.17% 1 > > । > । ■ H , 395 482 m/z-> 50 100 150 200 250 300 350 400 450 Abundance #71005: Ethanedioc acid, bis(trimethylsilyl) ester 73

m/z-> 5000

45

I 50 100 117 150 147

190 219 200 250 300 350 400 450 m/z 7 T7 - ■ ■ i • 33.80 34.00 34.20 34.40 34.60

'Abundance #58836: 9,12,15-Octadecatrienoic acid, 2,3-bis[(trimethylsi 73 33.80 34.00 34.20 34.40 34.60 147 m/z 355.0,5 14.77% 220 5000- 109 191 281

‘ I*’ 249 — .123 377 ,. 452 1 1 I ' m/z-> 50 100 150 200 250 300 350 400 450 33.80 34.00 34.20 34.40 34.60

30649.D GCMS1126.M Mon Jan 28 12:19:01 2002 Page 15

NYC-WTC_000004268