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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004266
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\JAN2 502\30649.D vial: 34 Acq On : 25 Jan 2002 9:55 pm Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 13 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

31.51 2.31 ug/1 1264890 Chrysene-dl2 32.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-1,1/1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 3 2-Hexenedioic/acid, bis (trimethylsi 288 C12H2404Si2 055494-10-5 23 4 Butanoic acid, 3-methyl-2-[(trimeth 262 CllH26O3Si2 055124-92-0 23 Abundance Scan 2883 (31.514 min): 30649.D (-) m/ z 72.95“ 100.00% I 73

5000 147 221 281 355 31.20 31.40 31.60 31.80 ' «0- 45 117 , 191 , 249., 1 . 327, [ ■-' I 10a" ' ' TrTTmm- 401 429 If*FIrIt m/z 147.00 41.19% m/z 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 147 31.20 31.40 31.60 31.80 l 221 m/z 221.05 24.16% I ' 281 327 , , 415... 519.561 ! m/z-> 50 100 150 200 250 300 350 400 450 500 550 ^Abundance #71005 Ethanedioic acid, bis(trimethy‘sily!; oster I 73 147 31.20 31.40 31.60 31.80 5000 m/z 281.00 15.67% 45 117 190 219 miz-> 50__ 100 150 200 250 300 350 400 450 500 550 Abundance #40777: 2-Hexenedioic acid, bis(trimethylsilyl) ester, (E)- 73 31.20 31.40 31.60 31.80 m/z 355.05 11.32% 5000 147 45

— 112 244 273 > । i • • ■ > । ■ 1 1 I ' 1 1 1 1 m/z—> 50 100 150 200 250 300 350 400 450 500 550 31.20 31.40 31.60 31.80

30649.D GCMS1126.M Mon Jan 28 12:18:52 2002 Page 13

NYC-WTC_000004266

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NYC-WTC_000004266Source: NYC Law Department, mirrored locally

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