NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\JAN2502\30649.D Vial: 34
Acq On : 25 Jan 2002 9:55 pm Operator: 209 GALOS
Sample : REINJECT Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 12 1-Monolinoleoylglycerol trimet Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
30.05 2.55 ug/1 1398210 Chrysene-dl2 32.80
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 42
2 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 27
3 3-Isopropoxy-1,1/1,7,7, 7-hexamethyl 576 C18H5207Si7 071579-69-6 25
4 1,1,1,5,7,7 ,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 23
Abundance Scan 2723 (30.045 min): 30649.D (-) m/ z 73.00 100.00%
1 73
5000-
147
221 I rrii
1...............
i 11 1 1 i11
| 281 355 429 29.80 30.00 30.20 30.40
0
45 117.^ 191 1 . 249. [ , 327 I 401 ---P
TTTTTuumuuumufT m/z 147.00
m/z->
Abundance
' -1 1 1
50 100 150 200 250 300 350 400 450 500 550
36.54%
#58871:1-Monolinoleoylglycerol trimethylsilyl ether
73
207
5000 147 ■ 1 i 1 ■ T1 1 1 1 1 1 i 1 1
103 ! 29.80 30.00 30.20 30.40
34
281 m/z 221.05 20.97%
m/z->
"II 1 1 1 1 1 ।
50 100 150 200
-L
250 300 350
395
400 450
482
500 550
Abundance #73975: Benzoic acid 2.4-bis[(trimethylsii oxyl- trip <:i
73
■ > 1 < ■ ■ ■ r ■ | 1 ■ ■ I | > ■
29.80 30.00 30.20 30.40
5000 355 m/z 355.05 14.16%
45
133 193 223 281
m/z- >
Abundance
50 100 150 200 250 300 350 400__ 450 500 550
—
#60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-i5,5-tris(trim IT
73 29.80 30.00 30.20 30.40
m/z 281.00 12.65%
5000
147
221
T 327 , 415 .... 519 561 —
m/z-> 50 100 150 200 250 300 350 400 450 500 550 29.80 30.00 30.20 30.40
30649.D GCMS1126.M Mon Jan 28 12:18:46 2002 Page 12
NYC-WTC_000004265
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