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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004265
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2502\30649.D Vial: 34 Acq On : 25 Jan 2002 9:55 pm Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 1-Monolinoleoylglycerol trimet Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

30.05 2.55 ug/1 1398210 Chrysene-dl2 32.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 42 2 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 27 3 3-Isopropoxy-1,1/1,7,7, 7-hexamethyl 576 C18H5207Si7 071579-69-6 25 4 1,1,1,5,7,7 ,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 23 Abundance Scan 2723 (30.045 min): 30649.D (-) m/ z 73.00 100.00% 1 73

5000- 147 221 I rrii 1............... i 11 1 1 i11 | 281 355 429 29.80 30.00 30.20 30.40 0 45 117.^ 191 1 . 249. [ , 327 I 401 ---P TTTTTuumuuumufT m/z 147.00 m/z-> Abundance ' -1 1 1 50 100 150 200 250 300 350 400 450 500 550 36.54% #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 ■ 1 i 1 ■ T1 1 1 1 1 1 i 1 1 103 ! 29.80 30.00 30.20 30.40 34 281 m/z 221.05 20.97%

m/z-> "II 1 1 1 1 1 । 50 100 150 200 -L 250 300 350 395 400 450 482 500 550 Abundance #73975: Benzoic acid 2.4-bis[(trimethylsii oxyl- trip <:i 73 ■ > 1 < ■ ■ ■ r ■ | 1 ■ ■ I | > ■ 29.80 30.00 30.20 30.40 5000 355 m/z 355.05 14.16% 45 133 193 223 281 m/z- > Abundance 50 100 150 200 250 300 350 400__ 450 500 550 — #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-i5,5-tris(trim IT 73 29.80 30.00 30.20 30.40 m/z 281.00 12.65% 5000 147 221 T 327 , 415 .... 519 561 — m/z-> 50 100 150 200 250 300 350 400 450 500 550 29.80 30.00 30.20 30.40

30649.D GCMS1126.M Mon Jan 28 12:18:46 2002 Page 12

NYC-WTC_000004265

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NYC-WTC_000004265Source: NYC Law Department, mirrored locally

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