GCMS analysis results, sample AD30936, January 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\ JAN2502\30936A.D Vial: 3 Acq On : 25 Jan 2002 11:09 am Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 3-1sopropoxy-1,1,1,7,7,7-hexam Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

31.52 0.32 ug/1 84412 Chrysene-dl2 32.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy-1,1,1/7, 7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 1 -Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 38 3 2-Hexenedioic acid, bis (trimethylsi 288 C12H2404Si2 055494-10-5 23 4 t rans - 3 - Hexen dioic acid, bis(trime 288 C12H2404Si2 000000-00-0 23 Abundance Scan 2884 (31.519 mln): 30936A.D (-) m/z 73. 100.00% 73

5000- 147 221 —14ti II 1’* PePrr 1h"t 11' 281 356 31.20 31.40 31.60 31.80

m/z-> 49 — 50 117 , * I > • ria 1 1 i 1 100 150 200 -27 02 m/z 147.00 250 ‘ ‘ 300 ‘ 350 400 450 500 550 4 0.56% Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000- 147 31.20 31.40 31.60 31.80 ‘ m/z 221.05 23.76% 221 21 327 415 i 519 561 • ■ i 1 • miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether i 73 31.20 31.40 31.60 ‘stsb 1 147 207 5000 m/z 281.10 14.96% 34 103 281 395 482 ! ‘ ■ i ■ • • • t ■1 f ‘ i 1 ■1 ■ । ‘ । 1 • ■ ■ । ■ । • I » j • « m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #40777:2-Hexenedioic acid, bis(trimethylsily!) ester, (E)- 111 • * ■ • ।1' • • i1 • • • । ■ t 73 31.20 31.40 31.60 31.80 rn/z 355.05 10.90% 5000 147 45 244 273 । ? . ;1 , ।112 , , 11., 1* i 1 ■ • ■ I • ‘ • I ■ ■ ' ' i • • ■ • i ■ 1 • 1 i • ' ‘ • i ■ • • ' i • • ' ■ i ■ 1 ■ ■ i 1 ■ • ' i ■ • ■ ■ । • 1 i • ' ■ ■ i m/z-> 50 100 150 200 250 300 350 400 450 500 550 31.20 31.40 31.60 31.80

30936A.D GCMS1126.M Fri Jan 25 12:24:31 2002 Page 12

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