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GC/MS analysis results for sample AD23260, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23260 conducted on October 12, 2001.

NYC-WTC_000088079–000088097

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088087
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0 901\23260.D Vial: 6 Acq On 9 Oct 2001 6:15 pm Operator: 209 GTkLOS Sample g c/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\MBS75K.L ********************************************************************* Peak Number 2 Butyl hexadecanoate Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 29.51 1.21 ug/1 231258 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butyl h^adecanoate 312 C2 0H4 0O2: 000000-00-0 35 2 1-Hexe?fe, 2-methyl- 98 C7H14 006094-02-6 27 3 Cyclopentanecarboxylic acid, 2-amin 129 C6H11NO2: 040482-05-1 23 4 l,.3>Hexanediol, 2-ethyl-________________ 146 C8H18O2 000094-96-2 23 Abundance Scan 2665 (29.506 min): 23260.D (-) 7m/z 56700 100.00% 53 I 5000 41 73 129 257 II, r It l.y .1. .1.43157171185199213 J 29.20 29.40 29.60 29.80 312 A—Y" T: , I I » » I I > i I r j 1 1 1 I I I , I 1 I 1 i I I j I I I I j I I i f I I I I I j 1 I I r I I 1 I I m/z 57.00 47.81% m/z~> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate 55

553 258 ■ - _ - .J r . f r. r . I I La - I ~ I 1 r I T-I-] 2j3.20 29.40 29,60 29.80 240 312 m/z 41.05 38.01% 129

I'''' I'' I' ‘' r ' I mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #1354:1-Hexene, 2-methyl- 55

41 29.20 29.40 29.60 29.80 5000 m/z 43.05 36.98% 27 70

uU 98 I'' ‘' I'''' I'''' I I ' ' ' ' 1 ' ' ' ' r ' ' ' 1 ' ' ' ' I ' ' ' ' I m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5212: Cyclopentanecarboxylic acid, 2-amino-, trans- ■’M 5^ 29.20 29.40 29.60 29.80 m/z 73700 29714% 5000

30 ' ' ' < I I ' I I I « I ' I I ' < I > I > • • > I « I • • I ' ' I > I < > ' I I • I I > I -pm-rj I ' ' ' ■nZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

23260.D NP091101.M Thu Oct 11 10:43:52 2001 Page 2

NYC-WTC_000088087

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NYC-WTC_000088087Source: NYC Law Department, mirrored locally

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