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GC/MS analysis results for sample AD22975, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22975 conducted on October 15, 2001, noting other unknown compounds.

NYC-WTC_000087644–000087658

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document LiiDrary Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0201\22975.D Vial: 11 Acq On 2 Oct 2001 11:53 pm Operator: 2 09 GTkLOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Butyl hexadecanoate Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 29.54 0.51 ug/1 69073 Chrysene-dl2 33.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butyl hesc^ecanoate 312 C2 0H40O2: 000000-00-0 52 2 Cyclopentanecarboxylic acid, 2-amin 129 C6H11NO2; 037910-65-9 35 3 Oxiran^ 2,3-bis(1-methylethyl)-, t 128 C8H16O 054644-32-5 32 4 1-He;xfene, 2-methyl- 98 C7H14 006094-02-6 27 ^bundanc^ Scan 2668 (29.536 min): 22975.D (-) m/z 56.00 100.00% 5S

5000 4 73 257

n/z-> Abundance 20 I'''' i'' 40 h

60 q? 129

80 100 120 140 160 180 200 220 240 260 280 300 #44549: Butyl hexadecanoate 312 xX- ' I " " I'' I. I 29.20 29.40 29.60 29.80 m/z 57.00 ft 41.28%

55

5000 258 A™, 29.20 29.40 29.60 29.80 240 312 34.93% 129 m/z43.05 I I 157171185 214 Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5218: Cyclopentanecarboxylic acid, 2-amino-, cis-

29.20 29.40 29.60 29.80 5000 m/z 41.05 33.44% 1

30 129 70 o. 100 ,1 , , I'''' I'''' 11 ' ‘' I'' >1 94 4- I ___________ I' r 1 11.. i. I. M 111 .111 ..,. I . 11. (I. I 11.11 ,1 ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5067: Oxirane, 2,3-bis(1-methylethyl)-, trans- A I Cl I / 55 29.20 29.40 29.60 29.80 41 “m/z 73700 31.52%

5000

J 113128 ‘n’ -n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

22975.D NP091101.M Mon Oct 15 08:21:27 2001 Page 4

NYC-WTC_000087654

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NYC-WTC_000087654Source: NYC Law Department, mirrored locally

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