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GC/MS analysis results for sample AD22975, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22975 conducted on October 15, 2001, noting other unknown compounds.

NYC-WTC_000087644–000087658

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document ocdicii k-uiiipouiiu Keporc

Data File C:\HPCHEM\1\DATA\OCT0201\22975.D Vial: 11 Acq On 2 Oct 2001 11:53 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Dotriacontane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 33.71 0.47 ug/1 63731 Chrysene-dl2 33.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dotriacontane 451 C32H66 000544-85-4 90K 2 Heneicosane 296 C21H44 000629-94-7 90 / 3 Pentatriacontane 493 C35H72 000630-07-9 90 / 4 Eicosane, 7-hexyl-__________________ 366 C26H54 055333-99-8 90^ Abundance Scan 3123 (33.714 min): 22975.D (-) m/z SYTOO 100.00% 5|7

5000 85

Ti/z-> Abundance Uw 50 100 150 200 227 250 #74491: Dotriacontane 281 300 350 400 450 33.40 33.60 33.80 34.00 m/z 71.10 69767%

[7

Tililil 85 1 33.40 33.60 33.80 34.00 m/z 4^705 66724% J j, ■ J96.............. 281............................ 4^ 450^ ■n/z-> 50 100 150 200 250 300 350 400 450 Abundance #42201: Heneicosane 57 Hl J, 85 33.40 33.60 33.80 34.00 5000 m/z 85705 42.47%

|113 , I / j J , 177, .. ............. 268, 296....................................... ' ' I •n/z-> 50 100 150 200 250 300 350 400 450 Abundance #58743: Pentatriacontane T-r-p-T 7 33.40 33.60 33.80 34.00 m/z 55.00 26771%

5000 85

•n/z-> 50 100 150 200 250 300 350 400 450 33.40 33.60 33.80 34.00

22975.D NP091101.M Mon Oct 15 08:21:29 2001 Page 5

NYC-WTC_000087655

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NYC-WTC_000087655Source: NYC Law Department, mirrored locally

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