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GC/MS analysis results for sample AD22657, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22657 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087363–000087378

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087377
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2801\22657.D Acq On : 29 Sep 2001 3:09 am Ope: ? GALOS Sample : gc/ms unknown Ins- ; VMS 209 Mise Mui' , 00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integr. Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************** Peak Number 4 1,4-Dichlorobenzene-d4 Concentrat ' R.T. EstConc Area Relative to ISTD 11.65 0.54 ug/1 69886 1,4-Dichlorobenzene-d4

Hit# of 5 Tentative ID MW MolForm Qual

1 1,4-Diclp^6robenzene-d4 150 C6C12D4 33-1 '53 2 Benzen^l,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 !'■

■••3-1 25 3 Benzehebutanoic acid, 3-nitro-.gamm 223 C10H9NO5 3ii-l 17 4 Bip^enylene 152 C12H8 ■■j-3 9 ^bundanc^ Scan 720 (11.649 min): 22657.D (-) m/z 143 1$0

5000 115 52 78 11.40 1 i; _ ''I ""I "''I"'J" "I" "I"' 4*^ r m/z 151 : 3 '."3 :'% n/z-> 30 40 50 60 70 80 90 100110120130140150160170180190200210220 Abundance #9593:1,4-Dichlorobenzene-d4 1$0

5000 115 11.4o' .■ 78 1 52 m/z 114 z 5%

■n/z-> 35 ... II,.y, 4, 30 40 50 60 70 80 90 100110120130140150160170180190200210220 p-rrrpTTq-

Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1$0

115 11.40 1 5000 52 78 m/z tT . 3"%

35 87 TTjrt lt|-nTi 1111111 m U " I ‘'I " ' 'I I I ‘' ”l •' ' I" " I" " I ■nfe-> 30 40 50 60 70 80 90 100110120130140150160170180190200210220 ^bundance #28308: Benzenebutanoic acid. 3-nitro-.gamma.-oxo- 1$0 11.40 1 r. r.)__ m/z 52 i 5000

56 104 76 92 122 134 159 206 223 TT+rvrrr ■n I " " I' " ' I' ‘ " I''' '''' r I " I" "I" " I"'' I" " I"' ‘ I' nZz-> 30 40 50 60 70 80 90 100110120130140150160170180190200210220 11.40

22657.D NP091101.M Fri Oct 05 14:43:38 2001 4

NYC-WTC_000087377

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NYC-WTC_000087377Source: NYC Law Department, mirrored locally

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