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GC/MS analysis results for sample AD22657, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22657 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087363–000087378

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2801\22657.D 16 Acq On : 29 Sep 2001 3:09 am Ops' •too GALOS Sample : gc/ms unknown Ins t 'X/MS 209 Mise Mui' 1.0 9 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integr. < Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L . **********************************************************-.•- * -*** Peak Number 3 2-Hexanol Concentrat;' nk 3 R.T. EstConc Area Relative to ISTD 6.74 0.52 ug/1 67587 1,4-Dichlorobenzene-d4 2 1 . ”9

Hit# of 5 Tentative ID MW MolForm Qual

1 2-Hexa:^1 102 C6H14O -93-7 78 2 2-Pe: ^nol, 4-methyl- 102 C6H14O -11-3 64 3 2-Ha :anol, (S) - 102 C6H14O •’8-0 43 4 2-Xeptanol, (S)- 116 C7H16O ,;3-i 40 'kbund^ce Scan 185 (6.738 min): 22657. D (-) m/z 39.09% 4b

41 69

nfe-> 10 15 20 25 30 35 40 45 50 55 .... I....... ........ m/z 60 65 70 75 80 85 90 95 ; % Abundance #63583:2-Hexanol 4b

5000 6.40 6.60 7 to___ __ m/z Xk.' lb . 95% 69 5558 I 8487 I 1111' I"" I... 11.... I... 11... I1111111111 nZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63547: 2-Pentanol. 4-methyl- 4b 6.40 _ etc 5000 m/T' 4 3' 2; : %!

n/z-> Abundance 10 15 20 X 27

25 30 35 40 ...... . 45 50 55 60 65 57

#1769; 2-Hexanol, (S)- 4b 69

70 75 80 8487

85 90 95 JJ6.40 m/z I6.6( T o

5000 I

AaAWzx.- 55 ? 8487 111.... I... 11.... II.... I.... I.... I. Tlfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.6C

22657.D NP091101.M Fri Oct 05 14:43:36 2001 Pane 3

NYC-WTC_000087376

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NYC-WTC_000087376Source: NYC Law Department, mirrored locally

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