VOC analysis results, sample AE12738, June 4 2002

NYC 9/11 Public Portal Document

Data File C:\HPCHEM\l\DATA\02june04\12739A.D Vial: 9 Acq On 4 Jun 2002 7:06 pm Operator: 201-wb Sample nyc Inst : GC/MS Ins Mise , Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP052902.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

PeaJc Number 3 6,7-Benzo-phenothiazine-5,5-di Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 22.67 0.03 ug/L 30889 CHL0R0BENZENE-D5 21.75 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 5 2 l,2-Dihydroanthra[l,2-d]thiazole-2, 281 C15H7NO3S 000000-00-0 5 3 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 5 4 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 5 Abundance Scan 1097 (22.672 min): 12739A.D (-) m/z 281.00 100.00% 2$1

5000

44 tX 22.40 22.60 22.80 23.00 m/z 282.00 26.88% -n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothia2ine-5,5-dioxide 2(11

5000 22.40 22.60 22.80 23.00 217 m/z 283.00 20.94%

Ti/z-> Abundance 40 60 80 102 118 ' I‘''I' 100 120 140 160 180 200 220 240 260 280 #39586: 1,2-Dihydroanthra[1,2-d]thiazole-2,6,11 -trione K 232 264 A

2*1

22.40 22.60 22.80 23.00 5000 m/z 43.85 0.32%

209 253 76 127 153 170 ' I ' ' ' I ''' ■ I ■ ■ I f 111 . I I . I . I I . ri I . iTi-p -n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39624: 3,6-Bis(N-dimethylamino)-9-ethylcarbazole 2((1 22.40 22.60 22.80 23.00

5000 266

141 208222236250 I ....... . .-Il , IA ,I ' I ' ' ' ‘ I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280

12739A.D HP052902.M Tue Jun 04 19:45:33 2002 Page 3

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