VOC analysis results, sample AE11905, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\02MAY22\11901F.D Vial: 11 Acq On : 23 May 2002 3:49 am Operator: 201-wb Sample : nyc; fb Inst ; GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peale Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 22:66 0.10 ug/L 68712 CHLOROBENZENE-D5 21.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 83 2 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 5 3 l,2-Dihydroanthra[l,2-d]thiazole-2, 281 C15H7NO3S 000000-00-0 5 4 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 5 Abundance Scan 1097 (22.661 min): 11901F.D (-) m/z 281.25 100.00% 2$1

liTilil

73 133 191 22.40 22.60 22.80 23.00 44 I I II m/z 282.25 25.46% -n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 21 1

5000 22.40 22.60 22.80 23.00 m/z 283.25 18.60% 73 133 207 I I 163177^®'' I 235249265 -n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothiazine-5.5-dioxide 2i!1

TTprr TT-p-r 22.40 22.60 22.80 23.00 553 m/z 133.15 10.71%

217 232 102118 189 r ' ‘' I'''' ixJpJv 264 I T-rp-t-TT-p-r -n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39586:1,2-Dihydroanlhra[1,2-d]thiazole-2,6,11 -trione 2!(1 22.40 22.60 22.80 23.00 m/z 73.05 9.36%

5000 209 253 76 127 . 153 170 ....... Ip' I' '' ' I ' ‘ ' I ' ' I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 22.40 22.60 22.80 23.00

11901F.D HP051702.M Thu May 23 09:15:57 2002 Page 2 NYC-WTC_000083543