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VOC analysis results, sample AE11905, May 2002

Machine-extracted title · confidence 95%

Laboratory report for volatile organic compounds in sample AE11905 analyzed on May 22, 2002.

NYC-WTC_000083395–000083562

Folder label: “524 5/22/02 - 5/23/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\02MAY22\11901F.D Vial: 11 Acq On : 23 May 2002 3:49 am Operator: 201-wb Sample : nyc; fb Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-(2-Acetylcyclopentylidene)cy Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

17.93 0.05 ug/L 27752 1,4-DIFLUOROBENZENE 15.07

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-(2-Acetylcyclopentylidene)cyclohe 207 C13H21NO 000000-00-0 9 . 2 Acetamide, N-[4-(trimethylsilyl)phe 207 CllH17NOSi 017983-71-0 7 3 Pyrido[2,3-d]pyrimidine, 4-phenyl- 207 C13H9N3 028732-75-4 5 4 N-Cyano-N',N’,N'',N''-tetramethyl-1 207 C8H13N7 074150-88-2 5 Abundance Scan 819 (17.928 min): 11901F.D (-) m/z 207.15 100.00% 207

'n/z-> Abundance TiTiX

44 ' I ' ' 40 ■X 60 80 100 120 140 #24635: N-(2-Acetylcyclopentylidene)cyclohexylamine 160 180 200 L 2(1)7 17.60 17.80 18-00 18'20 m/z 208.15 17.56%

164 124 TT-p-T I ‘ ' I 5000 17.60 17.80 18.00 18.20 150 m/z 96.20 16.94% 82 97

Ti/z-> Abundance 40 60 XU 80 100 120 140 #24586: Acetamide, N-[4-(trimethylsilyl)phenyl]- 160 180 200

192 2(1)7 —— 17.60 17.80 18.00 18.20 m/z 43.95 4.63% 150

■n/z--> 40 45 60 7,3 80 91 100 106 120 140 165 160 180 X 200 Abundance #24634: Pyrido[2,3-d]pyrimidine, 4-phenyl- 207 17.60 17.80 18.00 18.20

5000 179 77 , 103 152 126 'n/2-> 40 60 80 100 120 140 .1'.160 .......180 200

11901F.D HP051702.M Thu May 23 09:15:54 2002 Page 1

NYC-WTC_000083542

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NYC-WTC_000083542Source: NYC Law Department, mirrored locally

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