VOC analysis results, sample AE12279, May 2002

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Data File : C:\HPCHEM\l\DATA\02MAY23\12284.D Vial: 8 Acq On : 24 May 2002 12:11 am Operator: 201-wb Sample : nys Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number .2 N-(2-Acetylcyclopentylidene)cy Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

17.95 0.06 ug/L 43726 1,4-DIFLUOROBENZENE 15.10

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-(2-Acetylcyclopentylidene)cyclohe 207 C13H21NO 000000-00-0 9 2 Acetamide, N-[4-(trimethylsilyl)phe 207 CllH17NOSi 017983-71-0 7 3 Pyridot2,3-d]pyrimidine, 4-phenyl- 207 C13H9N3 028732-75-4 5 4 IH-Indole, 5-methyl-2-phenyl- 207 C15H13N 013228-36-9 5 Abundance Scan 821 (17.946 min): 12284.D (-) m/z 207.15 100.00% 207'

5000

17.60 17.80 18.00 18.20

Ti/z-> 44 40 60 ' 'so' 100 120 140 160 180 200 I m/z 208.15 20.67%

Abundance #24635: N-(2-Acetylcyclopentyiidene)cyclohexylamine 207

164 124

553 17.60 17.80 18.00 18.20 82 97 IIO 150 m/z 96.10 17.04% 192

•n/z-> 40 60 80 100 120 140 160 180 200 Abundance #24586: Acetamide, N-[4-(trimethylsilyl)phenyl]- 192 207

17.60 17.80 18.00 18.20 5000 m/z 209.15 13.72% 150

45 73 91 106 I 165 'n/z-> 40 60 80 100 120 140 160 180 200 Abundance #24634: Pyrido[2.3-d]pyrimidine, 4-phenyl- 207 17.60 17.80 18.00 18.20 m/z 44.00 4.67%

5000 179 77

■n/z-> .......... X 40 60 80 100 ,

120 140 , , , , , |............

160 180 200 17.60 17.80 18.00 18.20

12284.D HP051702.M Fri May 24 15:07:15 2002 Page 2

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