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VOC analysis results, sample AE11905, May 2002

Machine-extracted title · confidence 95%

Laboratory report for volatile organic compounds in sample AE11905 analyzed on May 22, 2002.

NYC-WTC_000083395–000083562

Folder label: “524 5/22/02 - 5/23/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\02MAY22\12155.D Vial: 8 Acq On : 23 May 2002 1:39 am Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peale Number 1 N-(2-Acetylcyclopentylidene)cy Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

17.93 0.05 ug/L 28143 1,4-DIFLUOROBENZENE 15.07

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-(2-Acetylcyclopentylidene )cyclohe 207 C13H21NO 000000-00-0 9 2 Hexahydropyridine, l-methyl-4-[4,5- 207 C12H17NO2 000000-00-0 9 3 Pyrido[2,3-d]pyrimidine, 4-phenyl- 207 C13H9N3 028732-75-4 5 4 IH-Indole, 2-methyl-3-pheny1- 207 C15H13N 004757-69-1 5 Abundance Scan 819 (17.928 min): 12155.D (-) m/z 207.15 100.00% 207

250

17.60 17.80 18.00 18.20 44 m/z 208.15 22.11% •n/z-> 40 60 80 1(30 12(3 ' 140 160 180 2(30 Abundance #24635: N-(2-Acetylcyclopentylidene)cyclohexylamine 207

164 124 -n-p-r-r-r-j-r 553 17.60 17.80 18.00 18.20 82 97 ’^0 150 m/z 96.10 16.92% 192 ' ' I ' HP m/z-> 40 60 80 100 120^^140^160^ 180 200 Abundance #24610: Hexahydropyridine, 1-methyl-4-[4,5-dihydroxyphenyl]- 2(1)7 70 42 97 Ui. T? 17.60 17.80 18.00 18.20 5000 m/z 44.00 7.99% 82 I 136 j JI....... 123 j 150 '............ I / L I . Ti/z-> 40 60 80 100 120 140 160 180 200 Abundance #24634: Pyrido[2.3-cl]pyrimidine. 4-phenyl- 2(1)7 17.60 17.80 18.00 18.20

5000 179 77 , 103 152 . ........ ,1...... ,l|, 126 Tl/z-> 40 60 80 100 120 140 160 180 200

12155:D HP051702.M Thu May 23 10:22:06 2002 Page 1

NYC-WTC_000083512

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NYC-WTC_000083512Source: NYC Law Department, mirrored locally

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