VOC analysis results, sample AE12737, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\O2JUNE3\12737D.D Vial: 7 Acq On 3 Jun 2002 8:44 pm Operator: 201-wb Sample 524; dup. Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP052902.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peale Number 2 Hexahydropyridine, l-methyl-4- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 17.95 0.03 ug/L 22395 1,4-DIFLUOROBENZENE 15.11 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexahydropyridine, l-methyl-4-[4,5- 207 C12H17NO2 000000-00-0 9 2 Pyridot2,3-d]pyrimidine, 4-phenyl- 207 C13H9N3 028732-75-4 5 3 IH-Isoindole-l, 3(2H)-dione, 2-butyl 207 C12H17NO2 054934-85-9 5 4 IH-Indole, l-methyl-2-phenyl-_______ 207 C15H13N 003558-24-5 5 Abundance Scan 820 (17.953 min): 12737D.D (-) m/z 207.05 100.00% 21 )7

5000 ,1,- >1,1 95 17.60 17.80 18.00 18.20 ■ 1^, , I , , , , I I . , I I I I I I I I I I I I I I I I I I I I I I I I I I m/z 207.95 21.14% Ti/z-> 40 60 80 100 120 140 160 180 200 Abundance #24610: Hexahydropyridine, 1-methyl-4-[4,5-dihydroxyphenyl]- 2(1)7 70 42 97 5000 “T T' 82 17.60 17.80 18.00 18.20 m/z 95.90 18.85% 136 123 ,1 150 192

Tl/Z-> 40 60 80 100 120 140 160 180 200 Abundance #24634: Pyrido[2,3-d]pyrimidine. 4-phenyl- 2(1)7 .......... A .......... , 17.60 17.80 18.00 18.20 5000 m/z 43.85 14.59% 179 77 , 103 .......I I........ ■ n/z-> 40 60 80 100 120 140 160 180 200 Abundance #24616: 1H-lsoindole-1,3(2H)-dione. 2-butyl-4,5,6,7-tetrahy 2(1)7 17.60 17.80 18.00 18.20 79

5000 165

r*-*|-T-n-n-T-yT— 111 124 136 -n/z-> 40 60 80 100 120 140 160 180 200

12737D.D HP052902.M Wed Jun 05 15:30:22 2002 Page 2

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