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VOC analysis results, sample AE12531, May 2002

Machine-extracted title · confidence 95%

Laboratory report for volatile organic compounds in sample AE12531 analyzed on May 24, 2002.

NYC-WTC_000083681–000083805

Folder label: “524 5/24/02 - 5/25/02

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Scanned page image, NYC-WTC_000083730
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\02may24\12533.D vial: 5 Acq On : 24 May 2002 7:32 pm Operator: 201-wb Sample : 524 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peale Number 2 Hexahydropyridine, l-methyl-4- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

18.00 0.04 ug/L 38588 1,4-DIFLUOROBENZENE 15.14

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexahydropyridine, l-methyl-4-[4,5- 207 C12H17NO2 000000-00-0 9 2 Cyclotrisiloxane, hexamethyl- 222 C6H18O3Si3 000541-05-9 9 3 Pyrido[2,3-d]pyrimidine, 4-phenyl- 207 C13H9N3 028732-75-4 5 4 cis-4-Ethoxy-.beta.-methyl-.beta.-n 207 C11H13NO3 000000-00-0 5 Abundance Scan 824 (17.997 min); 12533.D (-) m/z 207.15 100.00% 207

5000

17.60 17.80 18.00 18.20 18.40 m/z 208.15 24.12% lVz-> 40 ' ' ' ‘ 1 ' ' ' ‘ I ' ' ' ' r' ' ' ' I ' ' ' ' I ' ‘ 60 80 100 120 140 160 180 200 ' n Abundance #24610: Hexahydropyridine, 1-methyl-4-[4,5-dihydroxyphenyl]- 207 70 42

5000 97 i 17.60 17.80 18.00 18.20 18.40 82 m/z 209.25 19.26% 136 I 123 j 150.......... , , L , , m/z-> 40 60 80 100 120 140 160 180 200 Abundance #70586: Cyclotrisiloxane, hexamethyl- 207

I 17.60 17.80 18.00 18.20 18.40 m/z 96.10 16.45% 5000

75 .T, ■ I ' I ' ' ’ ' I ' m/z-> 40 60 80 100 120 140 160 180 200 Abundance #24634: Pyrido[2,3-d]pyrimidine, 4-phenyl- -rr-p-T 207 17.60 17.80 18.00 18.20 18.40 m/z 133.05 14.18%

553 179 77 103

tt/z-> .40........ 60 II,.80 100 120 140 160 180 200 17.60 17.80 18.00 18.20 18.40

12533.D HP051702.M Fri May 24 20:11:59 2002 Page 2

NYC-WTC_000083730

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NYC-WTC_000083730Source: NYC Law Department, mirrored locally

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