VOC analysis results, sample AE10890, May 2002

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Data File : C:\HPCHEM\l\DATA\02MAY07\0507Bl.D Vial: 1 Acq On : 7 May 2002 9:02 am Operator: 201-wb Sample : lab blank 1 (voc di) Inst : GC/MS Ins Mise : May 6, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP042202.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Pea)< Number 2 Hexahydropyridine, l-methyl-4- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

17.96 0.05 ug/L 28385 1,4-DIFLUOROBENZENE 15.10

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexahydropyridine, l-methyl-4-[4,5- 207 C12H17NO2 000000-00-0 9 2 Pyrido[2,3-d]pYrimidine, 4-phenyl- 207 C13H9N3 028732-75-4 5 3 Cyclohexane, 1,1'-(1,3-propanediyl) 208 C15H28 003178-24-3 4 4 Cyclohexanamine, N-cyclooctylidene- 207 C14H25N 054699-42-2 4 Abundance Scan 821 (17.962 min): 0507B1.D (-) m/z 207.15 100.00% 2(17 8553

6lililil

4000 "T 17.60 17.80 18.00 18.20 96 m/z 208.25 26.19% ■n/z-> 40 60 80 100 120 140 160 180 200 Abundance #24610: Hexahydropyridine. 1-methyl-4-[4,5-dihydroxyphenyl]- 207 70 42 97 5000 "T 17.60 17.80 18.00 18.20 82 m/z 96.00 21.27% 136 123 ,| 150 192 tVz-> 40 60 80 100 120 140 160 180 200 Abundance #24634: Pyrido[2,3-d]pyrimidine, 4-phenyl- 207

"T a. 17.60 17.80 18.00 18.20 5000 179 77

■n/z-> 40 I,. , 60 80 il... X....” 100 120 140 ....I.... 160 180 200 Abundance #24996: Cyclohexane, 1,1 '-(1,3-propanediyl)bis- 8t3

5000 55

67 208 96

Ti/z--> 40 60 80 X/ 100 109 125 120 140 160 180 180 200

0507B1.D HP042202.M Wed May 08 11:16:44 2002 Page 2

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