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VOC analysis results, sample AE10890, May 2002

Machine-extracted title · confidence 95%

Laboratory report for volatile organic compounds in sample AE10890 analyzed on May 7, 2002.

NYC-WTC_000083003–000083125

Folder label: “524 5/7/02 - 5/8/02

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Scanned page image, NYC-WTC_000083009
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\02MAY07\0507Bl.D vial: 1 Acq On : 7 May 2002 . 9:02 am Operator: 201-wb Sample : lab blank 1 (voc di) Inst : GC/MS Ins Mise : May 6, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP042202.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Azetidine, 1-(p-methoxybenzyl) Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

22.70 0.04 ug/L 26308 CHLOROBENZENE-D5 21.76

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Azetidine, 1-(p-methoxybenzyl)-3,3- 281 C19H23NO 022606-98-0 4 2 p-Trimethylsilyloxybenzaldehyde oxi 281 C13H23NO2Si2 000000-00-0 4 3 Phenol, 2,2'-[(1-methyl-l,2-ethaned 282 C17H18N2O2 000094-91-7 4 4 Benzenepropanamine, N-(1,1-dimethyl 281 C20H27N 015793-40-5 4 Abundance Scan 1099 (22.695 min); 0507B1.D (-) m/z 281.35 100.00% 2$1

8000

6553 22.40 22.60 22.80 23.00 4000 m/z 282.35 36.13% fTi/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39iratiii Azetidine, 1 -(p-methoxybenzyl)-3,3-dimethyl-2-pheny 1$1

5000 T 281 22.40 22.60 22.80 23.00

225 251 92 160 195 tX, -4^ I yf-n I' ''' I'''' I -n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39569: p-Trimethylsilyloxybenzaldehyde oxime, trimethylsil 7|5

5000 281 266

-n/z-> 45 ' I ' ' ' ' I ' ' XUS I 135 J 40 60 80 100 120 140 160 180 200 220 240 260 280 T 239 '' ' Xi Abundance #39799: Phenol, 2,2'-[(1-methyl-1,2-ethanediyl)bis(nitrilom 4l4

207 135 5000 77 107 149 281

-n/z-> 40 60 I'''' I £ I......... 80 100 120 140 160 180 200 220 240 260 280

0507B1.D HP042202.M Wed May 08 11:16:47 2002 Page 3

NYC-WTC_000083009

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NYC-WTC_000083009Source: NYC Law Department, mirrored locally

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