VOC analysis results, sample AE02089, Feb 7 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\02FEB06\2093.D • Vial: 6 Acq On 6 Feb 2002 8:07 pm Operator: 201-wb — Sample nyc Inst : GC/MS Ins— Mise Multiplr: 1.00 — MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Azetidine, 1-nitroso- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

15.53 0.04 ug/L 43857 1,4-DIFLUOROBENZENE 15.11

Hit# of 5 Tentative ID MW MolForm CAS# Qual—

1 Azetidine, 1-nitroso- 86 C3H6N20 015216-10-1 5 2 Ethanone, 1-oxiranyl- 86 C4H602 004401-11-0 5 3 2-Butanone, 3-methyl- 86 C5H10O 000563-80-4 4 4 2-Pentanone 86 C5H10O 000107-87-9 4 Abundance Scan 669 (15.531 min): 2093. D (-) m/ z 43.05 100.00% 4)3

5000 A ' ' l • • » • 1 • ■ > ' I • —— 39 । 86 15.20 15.40 15.60 15.80

niz-> mmmmTTTTTT q 20 25 30 35 40 4550556065 70 7580859095 m/z 41.15 21.54% Abundance #646: Azetidine, 1-nitroso- 33

41 5000 86 ■ ■ i ■ ■ ■ ■ i ■ i ■ ' ' ' i ■ ■ ■ ■ i 15.20 15.40 15.60 15.80 55 44 m/z 86.10 18.69%

niz-> 20 25 38 PP +— 30 35 40 TT T7H 52 + 69 i' ■ " i " ■' i ■ ■ ■ ■ i 45 50 55 60 65 70 75 80 85 90 95 ■ ■ i " “ i1 -ommihmne t Abundance #666: Ethanone, 1-oxiranyl- —an 43 ■ f i ■ ' 1 ‘ i ■ ■ ‘ • i ■ ■ ‘ • i ■ ■ ■ ■ i 15.20 15.40 15.60 15.80 5000 m/z 38.95 16.16% 27 55 71 86 31 39 — ' I' "H 1 ■ ■ i" ■ ■ i ■ ■ " i ■ ■ i ■' ■ ■ i ■ ■ i < • ■ ■ i ■ niz-> 20 25 30 35404550556065 70 75 80859095 Abundance #703:2-Butanone, 3-methyl- 43

5000

27 86

m/z—> —38,4 ■ ■ i ■ ■ ■ ■ i1 TTT 57 71 | Tmmmmmn;mdutman—au—nmanmuuTIT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 15.20 '15'40 15.60 15.80 ‘ 1

2093.D HP013102.M Wed Feb 06 21:22:01 2002 Page 2 — —

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