DEP document fragment, February 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\0 2 FEB05\2084.D Vial: 7 Acq On : 5 Feb 2002 10:40 pm Operator: 201-wb Sample : 524 nyc Inst : GC/MS Ins Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP020502.M (RTE Integrator) Title : VOCS BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Azetidine, 1-nitroso- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 15.90 0.03 ug/L 35169 1,4-DIFLUOROBENZENE 15.11 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Azetidine, 1-nitroso- 86 C3H6N20 015216-10-1 4 2 3-Pentanone 86 C5H10O 000096-22-0 4 3 2-Penten-1-ol, (E) - 86 C5H10O 001576-96-1 3 4 Azetidine 57 C3H7N 000503-29-7 3 Abundance Scan 689 (15.896 min): 2084.D (-) m/z 57.05 100.00% 57

5000

86 Q 39 42 a . L i ■ 11 > 15.60 15.80 16.00 16.20 ' ■ ■ i • ■ ■ ■ i ‘ • i'' " i ■ •'11 ■ ■ ‘111 ■ ■ • i1 ■ ■ ■ i ■ ’ 11 m/z 86.10 22.57% miz-> 20253035 40 4550556065 70 75 808590 95 Abundance 33 #646: Azetidine, 1-nitroso- N 41 5000 86 ■ ■ ■ i ■ 1 1 ■ i ‘ ■ ■ ■ i 1 1 1 1 i 1 1 1 1 1 15.60 15.80 16.00 16.20 44 55 m/z 42.15 14.87% 38 52 Il 69 ।" i ■ ■ ■ ■ i'" h 1"11"1' i"111 ■ |111 ‘ 111 ’11 ' ।1111111 ■ " i ■ " ■ i' niz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #723:3-Pentanone 23 57 ■ ‘ i ■ ■ ■ ■ i ‘ • ‘ i • ■ • ■ i 1 1 1 ‘ i 15.60 15.80 16.00 16.20 5000 m/z 38.95 13.29%

86 37 43 53 , ‘ ■ i' W • i ■ “ ■ i ‘11 ■ i “ “ i “ 1 ■ 11 1 ■ i" “ i■ “ ■i■11111111111111 11 ■ ■ ■11' miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #686:2-Penten-1-ol, (E)- 57 15.60 15.80 16.00 16.20 m/z 43.05 12.98%

/z—> 5000

20 25 27

31

TT-fT 30 44

mP I' ■''50I■■|1 ■! ,। 35 40 45 50 55 53 86 111 ■1 • > i > 11 > 11 < > ■ । < < 111 > 1111‘11111111111

60 65 67 71

70 75 80 85 90 95 1. 15.60 15.80 16.00 16.20

2084.D HP020502.M Thu Feb 14 10:54:49 2002 Page 1

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