SB1524 volatile analysis results, sample AE01938, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\02FEB04\01937F.D Vial: 13 Acq On 4 Feb 2002 7:09 pm Operator: 201-wb Sample : nyc fb Inst : GC/MS Ins Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Azetidine, 1-nitroso- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

15.58 0.04 ug/L 33581 1,4-DIFLUOROBENZENE 15.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Azetidine, 1-nitroso- 86 C3H6N20 015216-10-1 5 2 2-Butanone, 3-methyl- 86 C5H10O 000563-80-4 5 3 2-Pentanone 86 C5H10O 000107-87-9 4 4 Acetic acid ethenyl ester 86 C4H602 000108-05-4 4 Abundance Scan 672 (15.583 min): 01937F.D (-) m/z 43.05 100.00% 43

5000

miz-> ............ */ 20 25 30 35 40 ' i “ " I " '' i " “ i11 “ i " “ i' • " i' ■' ‘ i “ “ i " “ i ■ ■'' i ■ 45 50 55 60 65 70 75 80 86

85 90 95 v... 15.20 15.40 15.60 15.80 16.00 m/z 86.10 20.80% Abundance #646: Azetidine, 1-nitroso- 33

5000 41 86 ' ■ i ■ ■ . Q) 15.20 15.40 15.60 15.80 16.00 55 44 m/z 41.15 19.75% 38 52 - ■ ■ i ■ ■ ■ ■ i' ■ " " I'1111 TT-7H ■ ■ i ■ ■ ■ ■ i ■ N /z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62826:2-Butanone, 3-methyl- 43 15.20 15.40 15.60 15.80 16.00 5000 m/z 38.95 17.73% 86 27 Pmmmm39 111111111115511'111111111111711111 ■ i “ “ i1" ' i i ■ ■ I ■ ■ ■ ■ I ■■ m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62835:2-Pentanone AAg 43 15 20 15.40 15.60 15.80 16.00 m/z 43.95 11.02% / 5000

/z—> 27 ——— 11'■■■i■•'' i " ' i " " i ■ mmmmm T-rp- 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 58 71 86

15.20 15.40 15.60 15.80 16.00

01937F.D HP013102.M Tue Feb 05 09:37:15 2002 Page 2

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