SB1524 volatile analysis results, sample AE01938, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\1\DATA\02FEB04\01940.D Vial: 10 Acq On 4 Feb 2002 4:59 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCS BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Azetidine, 1-nitroso- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

15.58 0.04 ug/L 33422 1,4-DIFLUOROBENZENE 15.17

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Azetidine, 1-nitroso- 86 C3H6N20 015216-10-1 5 2 2-Butanone, 3-methyl- 86 C5H10O 000563-80-4 4 3 2-Pentanone 86 C5H10O 000107-87-9 4 4 2,3-Butanedione 86 C4H602 000431-03-8 3 Abundance Scan 671 (15.583 min): 01940.D (-) m/z 43.05 100.00% 43

5000 .... A. A—, 39 86 15.20 15.40 15.60 15.80 16.00 . - ' i ‘ ■ i ■' " i111 ■ i1' ‘ ‘ i1 ‘■ i “ “ i ■ •'' i' “ ' i ■''111 m/z 41.05 22.21% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #646: Azetidine, 1-nitroso- 33

41 5000 86 15.20 15.40 15.60 15.80 16.00 44 55 m/z 38.95 14.11% 38 52 miz-> TT-p-n-rp-r 20 25 11" I'1111 30 35 40 IT T7H 45 50 55 60 65 70 II....... A....... |.... 75 80 85 90 95 *11 “ 1' 1'

Abundance #703:2-Butanone, 3-methyl- 43 * 15.20 15.40 15.60 15.80 16.00 5000 m/ z 86.10 13.57%

27 86 57 71 | mz-> ........ | 20 25 130. 3538401 45 50 55 60 65 70 75 80 85 90 95 11' “ ■ i11' ■ i ■' ■ ■ i ■ ■ ■11 ■1 r' i11 ■' i “ “ i' “ ' i1 ■ ■ ■ i1 ■' III

Abundance #706:2-Pentanone "I 43 15.20 15.40 15.60 15.80 16.00 m/ z 44.00 10.10%

5000

27 3Q 86 , 5558 71 .. 1... *, 11'11111" '!11'' 111 " 111" I' " ■ i ■ ■ ■ ■ i ■ " ■ i' ■ ■ ■ i ■' ■ ■ i ■ miz—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 15.20 15.40 15.60 15.80 16.00

01940.D HP013102.M Tue Feb 05 09:42:32 2002 Page 2

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