NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\02FEB04\01940.D Vial: 10
Acq On 4 Feb 2002 4:59 pm Operator: 201-wb
Sample : nyc Inst : GC/MS Ins —
Mise : February 4, 2002 Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator)
Title : VOCs BY EPA METHOD 524
Library : C:\DATABASE\NBS75K.L
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Peak Number 3 2,4-lmidazolidinedione, 3-meth Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
15.83 0.04 ug/L 34748 1,4-DIFLUOROBENZENE 15.17
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2,4-lmidazolidinedione, 3-methyl- 114 C4H6N2O2 006843-45-4 3
2 1-(Propenylthio)prop-l-ene 114 C6H10S 000000-00-0 3
3 3-Cyclobutene-1,2-dione, 3,4-dihydr 114 C4H2O4 002892-51-5 2
4 Ethyl diazoacetate 114 C4H6N2O2 000623-73-4 2
Abundance Scan 685 (15.827 min): 01940.D (-) m/z 114.15 100.00%
114
5000
63 88
39 15.40 15.60 15.80 16.00 16.20
.... I...........
I ‘ 1 ‘ * I ' ' ' ' I ' * * ’ I ' ' ' ‘ I ' ' * 1 l 1 ‘ ' I 1 i ■ 1 ' ■ I ■ ■ ■ ■ i ' m/z 62.95 26.96%
n/z—> 20 30 40 50 60 70 80 90 100 110 120
Abundance #64088:2,4-lmidazolidinedione, 3-methyl-
1 4
58
5000
15.40 15.60 15.80 16.00 16.20
86 m/ z 88.00 23.50%
42 ri
71
' ■ ■ ■ i • ■ ■ ■ i ' 1
I 1 1 ' ' I ' ■ ■ ■ i ■ ■ ■ ' I ' ■
' 120 ‘
mJz~> 20 30 40 50 60 70 80 90 100 110
Abundance #2940:1-(Propenylthio)prop-1-ene
41 1 4
99
15.40 15.60 15.80 16.00 16.20
5000 m/z 38.95 14.43%
II
59 73 85
47
i ■ 1 * ‘ i 1 ■ • 1 i
- ■ i ■ • ■ ■ i 1 ■ • ■ i ■ ■ ■ ■ i ■ ■ ■ > i ■ -
m/z—> 20 30 40 50 60 70 80 90 100 110 120
Abundance #64087:3-Cyclobutene-1,2-dione, 3,4-dihydroxy- ■p-7
29 58 15.40 15.60 15.80 16.00 16.20
m/z 40.00 0.59%
5000 114
WWW
.... | 41 68 86
I * ' ' ' 1 ‘ ‘ ——— 1 । 1 ■ 1 1 । * * * ■ । ■ ■ 1 ■ । ■ ■ ■ ■ । ■ ■ ■ * । '
m/z—> 20 30 40 50 60 70 80 90 100 110 ' 120 ' 15.40 15.60 15.80 16.00 16.20
01940.D HP013102.M Tue Feb 05 09:42:34 2002 Page 3
NYC-WTC_000019282
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