SB1524 volatile analysis results, sample AE01938, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\02FEB04\01942F.D vial: 14 Acq On : 4 Feb 2002 7:52 pm Operator: 201-wb Sample : nyc fb Inst : GC/MS Ine Mise 2002 : February 4, Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Azetidine, 1-nitroso­ Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

15.93 0.03 ug/L 28647 1,4-DIFLUOROBENZENE 15.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Azetidine, 1-nitroso- 86 C3H6N2O 015216-10-1 7 2 Hexane 86 C6H14 000110-54-3 4 3 3-Pentanone 86 C5H10O 000096-22-0 4 4 2-Penten-l-ol, (E) -___________________ 86 C5H10O 001576-96-1 3 Abundance Scan 691 (15,931 min): 01942F.D (-) m/ z 100.00% 57

5000-

43 86 ■ ■ । ■ ■ ■ i ■ ■ ■ ■ i 15.60 15.80 16.00 16.20 - m/z 86.20 22.49% “ i''' ■ i'' " i'' ‘' i'''' i1''' i' ‘' i “ ■' i' tn/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #646: Azetidine, 1-nitroso- 33

41 5000 86 ’ I T 15.60 15.80 16.00 16.20 44 55 43.15 20.38%

m/z-> ■ ■ r ‘ 20 ■ i “ 25 30 "" !11111 35 38 40 T’ —7H+ 45 50 55 60 65 52 +- 69 11 1' " i “ “ i ■ “ ‘ i 70 75 80 85 '' i ‘ 90 ■ i • 95 Abundance #62873: Hexane 57 A HA 43 15.60 15.80 16.00 16.20 5000 m/z 42.05 19.44% 86 27 71 30 !>1111111111111 > ' ‘ ■ i ■ ‘ ■ ■ i • ■ ■ i ■ ■ " i ■' " i ■ i ■ ■ ■ ■ i ■ ' r ■ " i ■ ■ ■ ■ i m/z->_____ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62848:3-Pentanone 29 5(7 15.60 15.80 16.00 16.20 m/z 43.95 8.59% WMWWW 5000

86 26 42 1’1’4441 TH 1 ■ i ■ ■ “ i' “ ■ i ■ “ 11'1' ■ i “ ■ ■ i ■ ■ i1'' ■ 11 miz- > 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 15.60 15.80 16.00 16.20

01942F.D HP013102.M Tue Feb 05 09:50:35 2002 Page 4

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