VOC analysis results, sample AE12279, May 2002

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Data File C:\HPCHEM\1\DATA\O2MAY23\12286.D Vial 10 Acq On 24 May 2002 12:54 am Operator 201-wb Sample nys Inst GC/MS Ins Mise Multiplr 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★if

Peak Number 1 Hexahydropyridine, l-methyl-4- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

17.95 0.05 ug/L 38227 1,4-DIFLUOROBENZENE 15.10

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexahydropyridine, l-methyl-4-[4,5- 207 C12H17NO2 000000-00-0 9 , 2 Pyrido[2,3-d]pyrimidine, 4-phenyl- 207 C13H9N3 028732-75-4 5 3 4-Cyclohexene-l,2-dicarboximide, N- 207 C12H17NO2 028916-00-9 5 4 3,5-Ethanoquinolin-lO-one, decahydr 207 C13H21NO 021041-42-9 5 Abundance Scan 820 (17.945 min): 12286.D (-) m/z 207.15 100.00% 207

5000

■n" 17.60 17.80 18.00 18.20 ' I". .-1-'-.-'-^-. 'I.................... I'll" m/z 96.00 20.71% 'n/z-> 40 60 80 100 120 ' 140 160 180 200 Abundance #24610: Hexahydropyridine, 1-methyl-4-[4,5-dihydroxyphenyl]- 2(1)7 70 42 97 5000 -p-rr 17.60 17.80 18.00 18.20 82 m/z 208.15 19.02% 136 ,1 , 192

•n/z-> 40 60 80 100 120 140 160 180 200 Abundance #24634: Pyrido[2.3-d]pyrimidine, 4-phenyl- 207

17.60 17.80 18.00 18.20 m/z 209.15 13.74% 5000 179 77 , 103

Tl/z-> 40 60 80 100 120 140 160 180 200 Abundance #24614: 4-CycIohexene-1,2-dicarboximide, N-butyl-, cis- 2(1)7 80 17.60 17.80 18.00 18.20

5000 152 165

-n/z-> ' I ' ' ' ' I ' ' 40 60 80 100 120 140 -0 160 192 180 200 L

12286.D HP051702.M Tue May 28 09:15:08 2002 Page 1

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