VOC analysis results, sample AE11905, May 2002

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\02MAY22\12155.D Vial: 8 Acq On 23 May 2002 1:39 am Operator: 201-wb Sample nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peale Number 2 Cyclotetrasiloxane, octamethyl Concentration Ranle 1 R.T. EstConc Area Relative to ISTD R.T. 22.64 0.10 ug/L 67560 CHLOROBENZENE-D5 21.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 83 2 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 9 3 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 4 6,7-Benzo-phenothia2ine-5,5-dioxide 281 C16H11NO2S 000000-00:^5 /Abundance Scan 1096 (22.644 min): 12155.D (-) m/z 281.25 100.00% 2i 1

5000

73 133 193 265 22.40 22.60 22.80 23.00 44 I I II I m/z 282.35 30.07% •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966; Cyclotetrasiloxane, octamethyl- 2i 1

523 22.40 22.60 22.80 23.00 m/z 283.25 20.72% 73 133 207 I I 163177191 I 235249 265 ' I ‘ ' I ' ' ' ' I ' '' ' ' I ' ' ' ' I ' ' ' ' I ‘ ' tt/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39624; 3.6-Bis(N-dimethylamino)-9-ethylcarbazole 2) 1 ( T 22.40 22.60 22.80 23.00 5000 m/z 133.05 . 13.78% A 266

141 208222236 I ' I'''' I'''' I ■n/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643: Benzene, 1-phenyl-4-(2-cyano-2-phenylethenyl) 2$1 22.40 22.60 22.80 23.00 m/z 73.05 12.95% A 5000

253 126 203 I I I, ■ I ■ I 22423^8 1 H I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 22.40 22.60 22.80 23.00

12155.D HP051702.M Thu May 23 10:22:'09 2 002 Page 2

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