VOC analysis results, sample AE12531, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\02may24\12531F.D vial: 5 Acq On : 25 May 2002 1:17 am Operator: 201-wb Sample : 524; fb Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L *********************************************************** * * ******** Peale Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 22.70 0.09 ug/L 88160 CHLOROBENZENE-D5 21.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 78 2 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 9 3 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 4 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 5 Abundance Scan 1100 (22.695 min): 12531F.D (-) m/z 281.35 100.00% 2$1

aSE

■n/z--> 40 45 I 60 73 I 80 133 191 207 Il I I ' ' ' ' I ' 100 120 140 160 180 200 220 240 260 280 YI 22.40 22.60 22.80 23.00 m/z 282.25 30.15%

Abundance #41966: Cyclotetrasiloxane, octamethyl- 2$1

5000 22.40 22.60 22.80 23.00 m/z 283.35 20.81% 73 133 207 I 163177''9'’ ' I ' ' ' I 235343 365 I ' ' ' ' I ' '' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39624: 3,6-Bis(N-dimethylamino)-9-ethylcarbazole 2(11

22.40 22.60 22.80 23.00 WiW m/z 133.15 13.77% 266 A 141 208222236^^° ' I'''' I'''' I TT-p-T Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643: Benzene, 1-phenyl-4-(2-cyano-2-phenylethenyl) 2$1 22.40 22.60 22.80 23.00 m/z 73.05 13.51%

TiTiTil

126 I T I ■p" ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 22.40 22.60 22.80 23.00

12531F.D HP051702.M Sat May 25 01:56:45 2002 Page 3

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