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Volatile organic compound analysis results, sample AE08755, April 2002

Machine-extracted title · confidence 100%

Laboratory report listing volatile organic compounds and concentrations for sample AE08755 with method detection limit qualifiers.

NYC-WTC_000081917–000082000

Folder label: “524 4/11/02

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Scanned page image, NYC-WTC_000081922
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\O2APR11\O411B1.D Vial: 1 Acq On ; 11 Apr 2002 9:05 am Operator: 201-wb Sample : lb Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: rteint.p

Quant Method : C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : NBS75K.L ********************************************************************* Peale Number 1 Cyclotetrasiloxane, octamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 22.59 0.06 ug/L 62300 CHLOROBENZENE-D5 21.64 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 83 2 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 3 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 9 4 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-^9. Abundance Scan 1094 (22.594 min): 0411 Bl .D (-) m/z 281.35 100.00% 2$1

5000

22.20 22.40 22.60 22.80 23.00 45 73 133 191 265 m/z 282.35 27.41% -j-m-T I ' I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72646; Cyclotetrasiloxane, octamethyl- 2^1

5000 22.20 22.40 22.60 22.80 23.00 m/z 283.35 17.35%

45 59 73 I 133 177293207 235 265 L /I 'n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602; 6,7-Benzo-phenothiazine-5,5-dioxide 231 I''' ' 22.20 22.40 22.60 22.80 23.00 553 m/z 73.05 .13.32% A 217 I 232 102118 264 ' I'''' I -n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39624:3,6-Bis(N-dimethylamino)-9-ethylcarbazole 281 22.20 22.40 22.60 22.80 23.00 m/z 44.95 12.62%

552 266

141 208222236^1° I -n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 22.20 22.40 22.60 22.80 23.00

0411B1.D EC032902.M Mon Apr 15 16:05:16 2002 Page 1

NYC-WTC_000081922

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NYC-WTC_000081922Source: NYC Law Department, mirrored locally

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