VOC analysis results, sample AE12531, May 2002

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Data File C:\HPCHEM\l\DATA\02may24\12534.D Vial: 6 Acq On 24 May 2002 8:15 pm Operator: 201-wb Sample 524 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ♦ I****************-******************************************** ********

Pea)< Number 3 Cyclotetrasiloxane, octamethyl Concentration RanJe 2

R.T. EstConc Area Relative to ISTD R.T.

22.71 0.10 ug/L 78762 CHLOROBENZENE-D5 21.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 83 2 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 3 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 9 4 Benzene, l-phenyl-4-(2-cvano-2-phen 281 C21H15N 027869-56-3 9 lAbundance Scan 1100 (22.712 min): 12534.D (-) m/z 281.35 100.00% 2( 1

5000

133 22.40 22.60 22.80 23.00 73 191 265 I 1-^ m/z 282.25 28.62% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 2$1

lililil 22.40 22.60 22.80 23.00 m/z 283.35 16.75% 73 /l^ 163l77l?,lT 235219 265

■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothiazine-5,5-dioxide 2( II

22.40 22.60 22.80 23.00 m/z 133.05 12.92% A 217 I 232 102 118 264 I I ‘' I'''' I' T' ' ' ' I ' ll/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39624: 3,6-Bis{N-dimethylannino)-9-ethylcarbazole 21 1 22.40 22.60 22.80 23.00 m/z 191.20 10.12%

5000 266

141 250 208222236 , I 111,1 I'l I i'll, J Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 22.40 22.60 22.80 23.00

12534.D HP051702.M Fri May 24 20:55:19 2002 Page 3

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