VOC analysis results, sample AE12279, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\l\DATA\02MAY23\12287.D Vial: 11 Acq On 24 May 2002 1:37 am Operator: 201-wb Sample nys Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 22.70 0.11 ug/L 101690 CHLOROBENZENE-D5 21.78 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 74 2 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 3 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 5 4 lH-Indole-3-carboxaldehyde, 2-(1,1- 281 C19H23NO 025584-28-5 5 Abundance Scan 1100 (22.696 min): 12287.D (-) m/z 281.25 100.00% 21 1

5000

22.40 22.60 22.80 23.00 44 73 133 I 191 207 249 265 I m/z 282.25 30.87% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 2iH

5000 22.40 22.60 22.80 23.00 m/z 283.25 20.15% 133 207 73 163177 ■'9'' I 2352'^9 265 I I P ''' I ‘' I ' I ' ' ‘ I ' ' ' ' I ' '' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643: Benzene, 1-phenyl-4-(2-cyano-2-phenylethenyl) 2$1

22.40 22.60 22.80 23.00 5000 m/z 133.15 10.48%

253 126 I 2°^ I I I'''' I Ti/z-> Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 #39602: 6.7-Benzo-phenothiazine-5,5-dioxide 21 1 I 22.40 22.60 22.80 23.00 m/z 191.00 8.95% n 5000

217

K 232 102118 264 -n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 22.40 22.60 22.80 23.00

12287.D HP051702.M Tue May 28 09:16:13 2002 Page 3

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