VOC analysis results, sample AE12279, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\02MAY23\12287.D Vial: 11 Acq On 24 May 2002 1:37 am Operator: 201-wb Sample nys Inst : GC/MS Ins ■ Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Libratry : C:\DATABASE\NBS75K.L

Pea]< Number 2 Cyclotrisiloxane, hexamethyl- Concentration Ranlc 2

R.T. EstConc Area Relative to ISTD R.T.

17.95 0.05 ug/L 38129 1,4-DIFLUOROBENZENE 15.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotrisiloxane, hexamethyl- 222 C6H18O3Si3 000541-05-9 43 2 Hexahydropyridine, l-methyl-4-[4,5- 207 C12H17NO2 000000-00-0 9 3 Pyrido[2,3-d]pyrimidine, 4-phenyl- 207 C13H9N3 028732-75-4 5 4 Benzenamine, 4-bromo-2-chloro-_______ 205 C6H5BrClN 038762-41-3 5 Abundance Scan 821 (17.946 min): 12287.D (-) m/z 207.15 100.00% 2(17

5000

17.60 17.80 18.00 18.20

■n/z-> 40 60 80 96

100 120 140 160 180 200 I 191 m/z 208.25 26.11%

Abundance #70586: Cyclotrisiloxane, hexamethyl- 207

5000 17.60 17.80 18.00 18.20 m/z 96.10 19.70% 96 133 75 119 I 147 163 177 I ' I* ' ' '4 ' 'n/z--> 40 60 80 100 120 140 160 180 . 200 Abundance #24610: Hexahydropyridine. 1-methyl-4-[4.5-dihydroxyphenyl]- 2(1)7 70 42 17.60 17.80 18.00 18.20. 97 c m/z 191.10 16.74% 82 136 123 I 150 192

Tl/z-> 40 60 80 100 120 140 160 180 200 Abundance #24634: Pyrido[2,3-d]pyrimidine, 4-phenyl- 207 17.60 17.80 18.00 18.20 m/z 209.15 14.74%

5000 179 77 152 126 'n/z-> 40 60 80 100 120 140 . I'.160 ............ 180 ..... 200 ' I ' ' ' ' I ' ' I ' ' ' ' I ' ' ' ' I 17.60 17.80 18.00 18.20

12287.D HP051702.M Tue May 28 09:16:10 2002 Page 2

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